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페놀의 수산화 반응에 사용한 TS-1 촉매의 효과적인 재생 방법(소성 온도 의존성)
권송이 ( Song Yi Kwon ),윤성훈 ( Song Hun Yoon ),엄경섭 ( Kyung Sub Um ),이재욱 ( Jae Wook Lee ),이철위 ( Chul Wee Lee ) 한국화학공학회 2010 Korean Chemical Engineering Research(HWAHAK KONGHA Vol.48 No.6
In this study, calcination temperature dependence of TS-1 catalyst was investigated in the hydroxylation of phenol with hydrogen peroxide during the regeneration of catalyst. Catalyst was regenerated 5 times by calcining at 550˚C and 700˚C, respectively. When the catalyst was regenerated at 550˚C after 5th regeneration phenol conversion was decreased from 22.9% to 15.1% and at 700˚C after 5th regeneration phenol conversion was decreased from 22.9% to 18.8%. For formation ratio of catechol/hydroquinone was increased from 1.28 to 1.45 after 5th regeneration at 550˚C, and from 1.28 to 1.20 after 5th regeneration at 700˚C. The main reasons for deactivation of the catalyst were suggested by analyzing chemical/physical properties with XRD, UV-vis spectra, N2 adsorption/desorption and TGA, and evaluating the catalytic activity such as phenol conversion and product selectivity.