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      식품 중 아목시실린, 암피실린, 옥소린산 및 플루메퀸의 분석

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      https://www.riss.kr/link?id=A82754273

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      국문 초록 (Abstract)

      본 연구에서 확립한 분석법으로 총 393건의 시료를 분석한 결과 넙치에서 아목시실린 9건, 장어에서 옥소린산 4건과 플루메퀸 1건이 검출되었다. 아목시실린의 검출농도는 0.009-0.078 mg/kg의 범위를 나타내었고, 옥소린산의 검출농도는 0.02-0.20 mg/kg의 범위를 나타내었다. 플루메퀸은 잔류허용기준(0.5 mg/kg) 이하의 농도로 장어 1건(0.03 mg/kg)에서 검출되었다.
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      본 연구에서 확립한 분석법으로 총 393건의 시료를 분석한 결과 넙치에서 아목시실린 9건, 장어에서 옥소린산 4건과 플루메퀸 1건이 검출되었다. 아목시실린의 검출농도는 0.009-0.078 mg/kg의 범...

      본 연구에서 확립한 분석법으로 총 393건의 시료를 분석한 결과 넙치에서 아목시실린 9건, 장어에서 옥소린산 4건과 플루메퀸 1건이 검출되었다. 아목시실린의 검출농도는 0.009-0.078 mg/kg의 범위를 나타내었고, 옥소린산의 검출농도는 0.02-0.20 mg/kg의 범위를 나타내었다. 플루메퀸은 잔류허용기준(0.5 mg/kg) 이하의 농도로 장어 1건(0.03 mg/kg)에서 검출되었다.

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      다국어 초록 (Multilingual Abstract)

      The present study was performed to validate an analytical method for veterinary drugs, including amoxicillin, ampicillin, oxolinic acid and flumequin, in meat, fish, and their products as established in the 2007 Korea Food Code, and to monitor the respective drugs in 6 kinds of foods, namely beef, pork, flatfish, rockfish, freshwater eel and shrimp. Additionally, an HPLC-ESI-MS/MS method was developed for the qualification of these veterinary drugs. As a result of monitoring, these drugs were detected in 14 (3.6%) out of 393 samples. In particular, amoxicillin was detected in 9 flatfish samples, and oxolinic acid and flumequin were detected in 4 samples and 1 sample of freshwater eel, respectively. The detection levels of amoxicillin ranged from 0.009 to 0.078 mg/kg, in which 1 sample of flatfish contained more than the MRL (0.05 mg/kg). Flumequin detected in 1 sample of freshwater eel, was less than the MRL (0.5 mg/kg). Therefore, the majority of detected levels were less than the MRLs, with the exception of 2 samples showing amounts that were 1-2 times higher than the MRLs. The detected veterinary drugs were identified and confirmed by the HPLC-ESI-MS/MS method created in this study.
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      The present study was performed to validate an analytical method for veterinary drugs, including amoxicillin, ampicillin, oxolinic acid and flumequin, in meat, fish, and their products as established in the 2007 Korea Food Code, and to monitor the res...

      The present study was performed to validate an analytical method for veterinary drugs, including amoxicillin, ampicillin, oxolinic acid and flumequin, in meat, fish, and their products as established in the 2007 Korea Food Code, and to monitor the respective drugs in 6 kinds of foods, namely beef, pork, flatfish, rockfish, freshwater eel and shrimp. Additionally, an HPLC-ESI-MS/MS method was developed for the qualification of these veterinary drugs. As a result of monitoring, these drugs were detected in 14 (3.6%) out of 393 samples. In particular, amoxicillin was detected in 9 flatfish samples, and oxolinic acid and flumequin were detected in 4 samples and 1 sample of freshwater eel, respectively. The detection levels of amoxicillin ranged from 0.009 to 0.078 mg/kg, in which 1 sample of flatfish contained more than the MRL (0.05 mg/kg). Flumequin detected in 1 sample of freshwater eel, was less than the MRL (0.5 mg/kg). Therefore, the majority of detected levels were less than the MRLs, with the exception of 2 samples showing amounts that were 1-2 times higher than the MRLs. The detected veterinary drugs were identified and confirmed by the HPLC-ESI-MS/MS method created in this study.

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      목차 (Table of Contents)

      • Abstract
      • 서론
      • 재료 및 방법
      • 결과 및 고찰
      • 요약
      • Abstract
      • 서론
      • 재료 및 방법
      • 결과 및 고찰
      • 요약
      • 문헌
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      참고문헌 (Reference)

      1 Shin HC, "Veterinary drugs residue monitoring" 10 : 530-531, 2006

      2 Shin HC, "Survey of veterinary drugs" 9 : 438-439, 2005

      3 Song SO, "Simultaneous determination of residual tetracyclines in beef, pork, and chicken meats by high performance liquid chromatography" 18 : 343-352, 1994

      4 Natural Veterinary Research and Quarantine Service, "Quality assurance and further direction of meat and meat products"

      5 Jung YH, "Monitoring of antibiotic residues in foods" 9 : 414-415, 2005

      6 Wibawa JI, "Measurement of amoxicillin in plasma and gastric samples using high-performance liquid chromatography with fluorimetric detection" 774 : 141-148, 2002

      7 Korea Food and Drug Administration, "MRLs for veterinary drugs in foods"

      8 ACS Committee on Environmental Improvement, "Guidelines for data acquisition and data quality evaluation in environmental chemistry" 52 : 2242-2249, 1980

      9 Jung SC, "Establishment of control system of antibiotics for livestocks" 9 : 420-421, 2005

      10 Jung SC, "Establishment of control system of antibiotics for livestocks" 7 : 1113-1114, 2003

      1 Shin HC, "Veterinary drugs residue monitoring" 10 : 530-531, 2006

      2 Shin HC, "Survey of veterinary drugs" 9 : 438-439, 2005

      3 Song SO, "Simultaneous determination of residual tetracyclines in beef, pork, and chicken meats by high performance liquid chromatography" 18 : 343-352, 1994

      4 Natural Veterinary Research and Quarantine Service, "Quality assurance and further direction of meat and meat products"

      5 Jung YH, "Monitoring of antibiotic residues in foods" 9 : 414-415, 2005

      6 Wibawa JI, "Measurement of amoxicillin in plasma and gastric samples using high-performance liquid chromatography with fluorimetric detection" 774 : 141-148, 2002

      7 Korea Food and Drug Administration, "MRLs for veterinary drugs in foods"

      8 ACS Committee on Environmental Improvement, "Guidelines for data acquisition and data quality evaluation in environmental chemistry" 52 : 2242-2249, 1980

      9 Jung SC, "Establishment of control system of antibiotics for livestocks" 9 : 420-421, 2005

      10 Jung SC, "Establishment of control system of antibiotics for livestocks" 7 : 1113-1114, 2003

      11 Jung SC, "Establishment of control system of antibiotics for livestocks" 8-2 : 2223-2224, 2004

      12 Lee TS, "Establishment of antimicrobials management system for aquaculture" 8-2 : 2225-2226, 2004

      13 Lee TS, "Establishment of antimicrobials management system for aquaculture" 7 : 1115-1116, 2003

      14 Lee TS, "Establishment of antimicrobials management system for aquaculture" 9 : 422-423, 2005

      15 Heo GJ, "Diseases of aquaculture animals and prevention of drug residues" 7 : S7-S19, 1992

      16 Stolker AAM, "Analytical strategies for residue analysis of veterinary drugs and growth-promoting agents in food-producing animal-a review" 1067 : 15-53, 2005

      17 Jung MS, "A study on the consumption structure analysis of fishes"

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      학술지 이력

      학술지 이력
      연월일 이력구분 이력상세 등재구분
      2023 평가예정 해외DB학술지평가 신청대상 (해외등재 학술지 평가)
      2020-01-01 평가 등재학술지 유지 (해외등재 학술지 평가) KCI등재
      2010-11-23 학회명변경 영문명 : Korean Society Of Food Science And Biotechnology -> Korean Society of Food Science and Technology KCI등재
      2010-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2008-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2006-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2004-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2001-07-01 평가 등재학술지 선정 (등재후보2차) KCI등재
      1999-01-01 평가 등재후보학술지 선정 (신규평가) KCI등재후보
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      학술지 인용정보

      학술지 인용정보
      기준연도 WOS-KCI 통합IF(2년) KCIF(2년) KCIF(3년)
      2016 1.03 1.03 1.1
      KCIF(4년) KCIF(5년) 중심성지수(3년) 즉시성지수
      1.11 1.08 2.013 0.18
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