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      HPLC를 이용한 식품 중 아조디카르본아미드 분석 = Analysis of Azodicarbonamide in Food Products by High Performance Liquid Chromatography

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      https://www.riss.kr/link?id=A104488240

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      다국어 초록 (Multilingual Abstract)

      This study was conducted to establish a method to analyze azodicarbonamide (ADA) in wheat flour. A new method using high performance liquid chromatography (HPLC) was developed for the determination of ADA in wheat flour. The recovery rate was 91.93~97...

      This study was conducted to establish a method to analyze azodicarbonamide (ADA) in wheat flour. A new method using high performance liquid chromatography (HPLC) was developed for the determination of ADA in wheat flour. The recovery rate was 91.93~97.54%. The limit of detection for ADA was 0.02 mg/kg and the limit of quantification was 0.05 mg/kg. The monitoring results for ADA contents using the established methods showed that it was detected as the low value of 0.95 mg/kg in one of 51 flour samples (detection rate : 2%), but not detected in 59 bakery samples. The detected ADA level was suitable to its usage standard, compared to the standard (45 mg/kg). Although the detection rate was very low, the established analytical method of ADA will contribute to the management of ADA in processed foods such as wheat flour and bakery.

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      참고문헌 (Reference)

      1 Noonan G.O., "Ther determination of semicarbazide (N-aminourea) in commercial bread products by liquid chromatography-mass spectrometry" 53 : 4680-4685, 2005

      2 Dennis, M.J., "The effect of azodicarbonamide concentrations on ethyl carbamate concentrations in bread and toast" 14 : 95-100, 1997

      3 Dennis M.J., "The effect of azodicarbonamide concentrations on ethyl carbamate concentrations in bread and toast" 14 : 95-100, 1997

      4 Mulder P.P.J., "The determination of biurea: A novel method to discriminate between nitrofuran and azodicarbonamide use in food products" 586 : 366-373, 2007

      5 Mulder, P.P.J., "The determination of biurea : A novel method to discriminate between nitrofuran and azodicarbonamide use in food products" 586 : 366-373, 2007

      6 Stadler, R.H., "Semicarbazide is a minor thermal decomposition product of azodicarbonamide used in the gaskets of certain food jars" 129 : 276-281, 2004

      7 Becalski, A., "Semicarbazide in Canadian bakery products" 23 : 107-109, 2006

      8 Becalski, A., "Semicarbazide formation in azodicarbonamide treated flour - A model study" 52 : 5730-5734, 2004

      9 Becalski A., "Semicarbazide formation in azodicarbonamide treated flour - A model study" 52 : 5730-5734, 2004

      10 de la Calle, M.B., "Semicarbazide - occurrence in food products and state-of-the-art in analytical methods used for its determination" 382 : 968-977, 2005

      1 Noonan G.O., "Ther determination of semicarbazide (N-aminourea) in commercial bread products by liquid chromatography-mass spectrometry" 53 : 4680-4685, 2005

      2 Dennis, M.J., "The effect of azodicarbonamide concentrations on ethyl carbamate concentrations in bread and toast" 14 : 95-100, 1997

      3 Dennis M.J., "The effect of azodicarbonamide concentrations on ethyl carbamate concentrations in bread and toast" 14 : 95-100, 1997

      4 Mulder P.P.J., "The determination of biurea: A novel method to discriminate between nitrofuran and azodicarbonamide use in food products" 586 : 366-373, 2007

      5 Mulder, P.P.J., "The determination of biurea : A novel method to discriminate between nitrofuran and azodicarbonamide use in food products" 586 : 366-373, 2007

      6 Stadler, R.H., "Semicarbazide is a minor thermal decomposition product of azodicarbonamide used in the gaskets of certain food jars" 129 : 276-281, 2004

      7 Becalski, A., "Semicarbazide in Canadian bakery products" 23 : 107-109, 2006

      8 Becalski, A., "Semicarbazide formation in azodicarbonamide treated flour - A model study" 52 : 5730-5734, 2004

      9 Becalski A., "Semicarbazide formation in azodicarbonamide treated flour - A model study" 52 : 5730-5734, 2004

      10 de la Calle, M.B., "Semicarbazide - occurrence in food products and state-of-the-art in analytical methods used for its determination" 382 : 968-977, 2005

      11 de la Calle M.B, "Semicarbazide - occurrence in food products and state-of-the-art in analytical methods used for its determination" 382 : 968-977, 2005

      12 "Korea Food and Drug Administration: Food Standards Code. Korean Foods Industry Association, Seoul, Korea (2008)"

      13 "Korea Food and Drug Administration: Food Additives Code. Korean Foods Industry Association, Seoul, Korea, pp 233-234 (2009)"

      14 Pereira, A.S., "Implications of the use of semicarbazide as a metabolic target of nitrofurazone contamination in coated products" 21 : 63-69, 2004

      15 ICH (International Conference on Harmonisation of Technical Requirements for Registration of Pharmaceuticals for Human Use), "ICH Topic Q2 (R1). Validation of analytical procedures: Text and methodology" European Medicines Agency

      16 Osborne, B.G., "High performance liquid chromatography of azodicarbonamide" 368 : 401-404, 1986

      17 Food and Agriculture Organization of United Nations, "FAO Nutrition Meetings Report (1966). Series 40, A, B, C"

      18 Canas, B.J., "Ethyl carbamate levels resulting from azodicarbonamide use in bread" 14 : 89-94, 1997

      19 Weak E.D., "Determination of azodicarbonamide in wheat flour" 53 : 881-889, 1976

      20 Weak, E.D., "Determination of azodicarbonamide in wheat flour" 53 : 881-889, 1976

      21 Food and Agriculture Organization of United Nations, "Combined Compendium of Food Additive Specifications - Azodicarbonamide" FAO 2006

      22 라임정, "Azodicarbonamide를 첨가한 밀가루 반죽의 물성 및 냉동저장 중 제빵 특성의 변화" 한국식품영양과학회 33 (33): 1566-1572, 2004

      23 National Institute of Food and Drug Safety Evaluation, "Analysisof food additives in foods" 2009

      24 de Stefanis, V.A., "Analysis of azodicarbonamide in wheat flour by liquid chromatography" 65 : 52-55, 1988

      25 Conant, J.B., "A quantitative study of semicarbazone formation" 54 : 2881-2899, 1932

      26 United States Food and Drug Administration, "21CFR172. 806. Azodicarbonamide"

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      학술지 이력

      학술지 이력
      연월일 이력구분 이력상세 등재구분
      2026 평가예정 재인증평가 신청대상 (재인증)
      2020-01-01 평가 등재학술지 유지 (재인증) KCI등재
      2017-01-01 평가 등재학술지 유지 (계속평가) KCI등재
      2013-01-01 평가 등재학술지 유지 (등재유지) KCI등재
      2010-01-01 평가 등재학술지 선정 (등재후보2차) KCI등재
      2009-01-01 평가 등재후보 1차 PASS (등재후보1차) KCI등재후보
      2008-01-01 평가 등재후보 1차 FAIL (등재후보1차) KCI등재후보
      2006-07-21 학회명변경 영문명 : The Korean Sociery Of Food Hygiene And Safety -> The Korean Society of Food Hygiene and Safety KCI등재후보
      2006-01-01 평가 등재후보학술지 선정 (신규평가) KCI등재후보
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      학술지 인용정보

      학술지 인용정보
      기준연도 WOS-KCI 통합IF(2년) KCIF(2년) KCIF(3년)
      2016 0.45 0.45 0.48
      KCIF(4년) KCIF(5년) 중심성지수(3년) 즉시성지수
      0.49 0.49 0.726 0.08
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