The synthesis of polyamic acid was studied to get optimized conditions. The spectrum of the product of reaction containing azobenzene chromophres was investigated by using ultraviolet spectrophotometry in various solvent at room temperature. Recrystal...
The synthesis of polyamic acid was studied to get optimized conditions. The spectrum of the product of reaction containing azobenzene chromophres was investigated by using ultraviolet spectrophotometry in various solvent at room temperature. Recrystallization of reaction product in ethanol solvent atomosphere results 73.2% monomer, 78.6% anhydride tetracarbonic acid, and 96% polyamic acid.
Maxwell displacement current(MDC)measuring technique has been applied on the study of monolayers of polyamic acid. The displacement current was generated from monolayers on the water surface by monolayer compression and expansion. Displacement current was generated when the area per molecule was about 250Ųand 120Ų. The charge flow and Maxwell displacement currents were investigated in connection with monolayer compression cycles. It was found that The maximum of MDCs appeared at the molecular area just before the initial rise of surface pressure in both 1st and 2nd compression cycles.