Methods in enzymology . 193 , Mass spectrometry ed. by James A. McCloskey

목차 (Table of Contents)

• CONTENTS
• CONTRIBUTORS TO VOLUME 193 = ⅸ
• PREFACE = xiii
• VOLUMES IN SERIES = xv
• Section I. General Techniques
• 1. Methods of Ionization / ALEX G. HARRISON ; ROBERT J. COTTER = 3
• 2. Mass Analyzers / KEITH R. JENNINGS ; GREGORY G. DOLNIKOWSKI = 37
• 3. Detectors / SYD EVANS = 61
• 4. Selected-Ion Measurements / J. THROCK WATSON = 86
• 5. Liquid Chromatography-Mass Spectrometry / MARVIN L. VESTAL = 107
• 6. Tandem Mass Spectrometry: Multisector Magnetic Instruments / MICHAEL L. GROSS = 131
• 7. Tandem Mass Spectrometry: Quadrupole and Hybrid Instruments / RICHARD A. YOST ; ROBERT K. BOYD = 154
• 8. Matrix Selection for Liquid Secondary Ion and Fast Atom Bombardment Mass Spectrometry / EDWIN DE PAUW = 201
• 9. Continuous-Flow Fast Atom Bombardment Mass spectrometry / RICHARD M. CAPRIOLI ; WILLIAM T. MOORE = 214
• 10. Collision-Induced Dissociation / ROGER N. HAYES ; MICHAEL L. GROSS = 237
• 11. Principles of Californium-252 Plasma Desorption Mass Spectrometry Applied to Protein Analysis / RONALD D. MACFARLANE = 263
• 12. Mass Spectrometry of Peptides and Proteins by Matrix-Assisted Ultraviolet Laser Desorption／Ionization / FRANZ HILLENKAMP ; MICHAEL KARAS = 280
• 13. Utility of Exact Mass Measurements / KLAUS BIEMANN = 295
• 14. Selection and Use of Mass Reference Standards / RICHARD M. MILBERG = 305
• 15. Chemical Derivatization for Mass Spectrometry / DANIEL R. KNAPP = 314
• 16. Introduction of Deuterium by Exchange for Measurement by Mass Spectrometry / JAMES A. MCCLOSKEY = 329
• 17. Preparation of Labeled Molecules by Exchange with Oxygen-18 Water / ROBERT C. MURPHY ; KEITH L. CLAY = 338
• Section II. Peptides and Proteins
• 18. Peptides and Proteins: Overview and Strategy / KLAUS BIEMANN = 351
• 19. Enzymatic and Chemical Digestion of Proteins for Mass Spectrometry / TERRY D. LEE ; JOHN E. SHIVELY = 361
• 20. Strategies for Locating Disulfide Bonds in Proteins / DAVID L. SMITH ; ZHONGRUI ZHOU = 374
• 21. Reversed-Phase High-Performance Liquid Chromatography for Fractionation of Enzymatic Digests and Chemical Cleavage Products of Proteins / KATHRYN L. STONE ; JAMES I. ELLIOTT ; GLENN PETERSON ; WALTER MCMURRAY ; KENNETH R. WILLIAMS = 389
• 22. Electrospray Ionization Mass Spectrometry / CHARLES G. EDMONDS ; RICHARD D. SMITH = 412
• 23. Sample Preparation for Plasma Desorption Mass Spectrometry / PETER ROEPSTORFF = 432
• 24. Molecular Weight Analysis of Proteins / IAN JARDINE = 441
• 25. Sequencing of Peptides by Tandem Mass Spectrometry and High-Energy Collision-Induced Dissociation / KLAUS BIEMANN = 455
• 26. Liquid Secondary Ion Mass Spectrometry of Phosphorylated and Sulfated Peptides and Proteins / BRADFORD W. GIBSON ; PHILIP COHEN = 480
• 27. Ientification of Attachment Sites and Structural Classes of Asparagine-Linked Carbohydrates in Glycoproteins / STEVEN A. CARR ; JOHN R. BARR ; GERALD D. ROBERTS ; KALYAN R. ANUMULA ; PAUL B. TAYLOR = 501
• 28. Characterization of Recombinant Proteins / HUBERT A. SCOBLE ; STEPHEN A. MARTIN = 519
• Section III. Glycoconjugates
• 29. Glycoconjugates: Overview and Strategy / ROGER A. LAINE = 539
• 30. Linkage Analysis Using Lindberg Method / CARL G. HELLERQVIST = 554
• 31. Linkage Analysis Using Reductive Cleavage Method / GARY R. GRAY = 573
• 32. Linkage Positions in Glycoconjugates by Periodate Oxidation and Fast Atom Bombardment Mass Spectrometry / ANNE-SOPHIE ANGEL ; BO NILSSON = 587
• 33. Tandem Mass Spectrometry in Structural Characterization of Oligosaccharide Residues in Glycoconjugates / WILHELM J. RICHTER ; DIETER R. M$$\ddot U$$LLER ; BRUNO DOMON = 607
• 34. Mass Spectrometry of Mixtures of Intact Glycosphingolipids / BO E. SAMUELSSON ; WESTON PIMLOTT ; KARL-ANDERS KARLSSON = 623
• 35. Preparation and Desorption Mass Spectrometry of Permethyl and Peracetyl Derivatives of Oligosaccharides / ANNE DELL = 647
• 36. Desorption Mass Spectrometry of Oligosaccharides Coupled with Hydrophobic Chromophores / LINDA POULTER ; A. L. BURLINGAME = 661
• 37. Oligosaccharide Characterization with High-Energy Collision-Induced Dissociation Mass Spectrometry / BETH L. GILLECE-CASTRO ; A. L. BURLINGAME = 689
• 38. Desorption Mass Spectrometry of Glycosphingolipids / JASNA PETER-KATALIN$$\acute I$$C ; HEINZ EGGE = 713
• 39. High-Mass Gas Chromatography-Mass Spectrometry of Permethylated Oligosaccharides / GUNNAR C. HANSSON ; HASSE KARLSSON = 733
• 40. Tandem Mass Spectrometry of Glycolipids / CATHERINE E. COSTELLO ; JAMES E. VATH = 738
• Section IV. Nucleic Acid Constituents
• 41. Constituents of Nucleic Acids: Overview and Strategy / JAMES A. MCCLOSKEY = 771
• 42. Preparation and Enzymatic Hydrolysis of DNA and RNA for Mass Spectrometry / PAMELA F. CRAIN = 782
• 43. Preparation of Trimethylsilyl Derivatives of Nucleic Acid Components for Analysis by Mass spectrometry / KARL H. SCHRAM = 791
• 44. Analysis of RNA Hydrolyzates by Liquid Chromatography-Mass Spectrometry / STEVEN C. POMERANTZ ; JAMES A. MCCLOSKEY = 796
• 45. Electron Ionization Mass Spectra of Trimethylsilyl Derivatives of Nucleosides / JAMES A. MCCLOSKEY = 825
• 46. Gas Chromatography-Mass Spectrometry of Free Radical-Induced Products of Pyrimidines and Purines in DNA / MIRAL DIZDAROGLU = 842
• 47. Analysis of 5-Methylcytosine in DNA by Isotope Dilution Gas Chromatography-Mass Spectrometry / PAMELA F. CRAIN = 857
• Appendixes
• 1. Mass and Abundance Values / JAMES A. MCCLOSKEY = 869
• 2. Reference Ions for Exact Mass Measurements / RICHARD M. MILBERG = 870
• 3. Mass Spectra of Matrix Materials / C. E. COSTELLO = 875
• 4. Calculation of Isotopic Abundance Distributions / JAMES A. MCCLOSKEY = 882
• 5. Nomenclature for Peptide Fragment Ions (Positive Ions) / KLAUS BIEMANN = 886
• 6. Residue Mass for Peptides / KLAUS BIEMANN = 888
• AUTHOR INDEX = 889
• SUBJECT INDEX = 915