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Elucidating synthesis of noble metal nanoparticles/graphene oxide in freescavenger γ-irradiation
Jie Shi,Wanwei Jiang,Liangsen Liu,Miaolei Jing,Fengyan Li,Zhiwei Xu,Xing-xiang Zhang 한국물리학회 2019 Current Applied Physics Vol.19 No.7
Three representative noble metal (Ag, Au and Pt) nanoparticles decorated graphene oxide (NMNPs/GO) composites were fabricated via γ-irradiation without scavenger. The NMNPs/GO composites exhibited the pure and well-dispersed particles structure, which directly illustrated that the GO could be acted as scavenger to benefit reduction and growth of NMNPs. Compared with irradiated GO (IGO), the GO substrate of composites had the lower relative content of hydroxyl groups, meanwhile, the relative contents of carbonyl groups (Pt > Au > Ag) were increased with increasing valence of noble metal. Such results illustrated that the abundant hydroxyl groups could convert the hydrated electrons, hydroxyl and hydrogen radicals to promote the growth of NMNPs on the surface of GO. In addition, the Raman signals of Ag NPs/GO composites were significantly enhanced (6.18 fold more than pristine GO, respectively), exhibiting obvious surface-enhanced Raman scattering activity. Therefore, this paper revealed that the GO could convert the hydrated electrons and radicals to synthetizing NMNPs/GO composites during γ-ray irradiation.
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Changrong Liu,Hongbin Tan,Aiguo Zheng,Xiangmei Kang,Ao Jiang,Rui Fang,Haorong Ren,Wanwei Fang 한양대학교 세라믹연구소 2020 Journal of Ceramic Processing Research Vol.21 No.3
The manufacture of sodium sulfide through a carbon reduction process, using sodium sulfate as raw material, generatessodium sulfide by-product sediment, which has potential health and environmental impacts. Herein, a novel strategy isproposed to recover sodium oxide from the sediment by using acidic treatment and the influence of solution pH on sodiumoxide content is systematically studied. The results reveal that the sodium oxide content decreases with decreasing pH valueof the solution. At pH = 4, the as-treated sediment results in Na2O content of 3.10 wt. %, which recovery rate is about 90%. Furthermore, the influences of sintering temperature and time on compressive strength and bulk density are studied. Ingeneral, the compressive strength and bulk density increase with increasing sintering temperature and time. After sinteringat 1,300 oC for 120 min, the compressive strength and bulk density of the sintered porous ceramic are 26.66 MPa and 1.31 g/cm3, respectively. The porous ceramic, sintered at 1,300 oC, mainly consists of hauyne, gehlenite and hematite phases. Insummary, the few flaws in cell-walls result in high compressive strength of the as-prepared porous ceramics.
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