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A new error bound estimate for linear complementarity problems of B-matrices
Jiaxian Huang,Hongmin Mo 한국전산응용수학회 2021 Journal of Applied and Pure Mathematics Vol.3 No.5
In this paper, the error bound for linear complementarity problems of B-matrices was studied, and a new estimate of the error bound has been obtained by using the range for the infinity norm of inverse matrix of strictly diagonally dominant M-matrices and applying the scaling technique of inequality. Theoretical analysis and numerical examples show that the new estimate is better than some previous results.
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Top-emitting organic light-emitting devices based on silicon substrate using Delta -doping technique
Zhijun Wu,Hengqun Guo,Jiaxian Wang 한국물리학회 2011 Current Applied Physics Vol.11 No.2
We have fabricated a Top-emitting organic light-emitting device on silicon substrate Delta -doping technique. Using ultrathin quinacridone as emitting layer, the performance of Top-emitting organic lightemitting device is improved obviously. However, when increasing the thickness of the anode, the performance of device is enhanced dramatically. The max power efficiency of device is 5.9 Lm/W at 5 V corresponding to the current efficiency of 9.3 cd/A. The max current efficiency of device is also increases to 11 cd/A at 7 V.
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Yanjun Li,Yanyang Wu,Jiawen Zhu,Jiaxian Liu 한국생물공학회 2012 Biotechnology and Bioprocess Engineering Vol.17 No.2
Biochemical 2,3-butanediol is a renewable material with the potential to be used as an alternative fuel. However, in the lack of an effective separation process has limited its industrial application. In this paper, an effective process was achieved to separate 2,3-butanediol by reactive-extraction. Acetaldehyde and cyclohexane were chosen as the reactant and extractant, respectively. Ion-exchange resin HZ732 was used as the catalyst. Reaction equilibrium and a kinetic study on the reaction between 2,3-butanediol and acetaldehyde were investigated to provide basic data for process development. The reaction enthalpy and activation energy of reaction of 2,3-butanediol and acetaldehyde were −30.05 ± 1.62 KJ/mol and 45.29 ± 2.89 KJ/mol,respectively. Feasible conditions were obtained as follows:operating temperature = 20℃, acetaldehyde: 2,3-butanediol = 0.5:1 (w/w), cyclohexane: fermentation broth = 0.5:1 (w/w), catalyst amount = 100 g/L, stirring rate = 500 rpm and three-stage counter-current extraction method was used. Under these conditions, the total yield rate of 2,3-butanediol from fermentation broth was over 90% and the mass fraction of 2,3-butanediol in the final product reached 99%. Biochemical 2,3-butanediol is a renewable material with the potential to be used as an alternative fuel. However, in the lack of an effective separation process has limited its industrial application. In this paper, an effective process was achieved to separate 2,3-butanediol by reactive-extraction. Acetaldehyde and cyclohexane were chosen as the reactant and extractant, respectively. Ion-exchange resin HZ732 was used as the catalyst. Reaction equilibrium and a kinetic study on the reaction between 2,3-butanediol and acetaldehyde were investigated to provide basic data for process development. The reaction enthalpy and activation energy of reaction of 2,3-butanediol and acetaldehyde were −30.05 ± 1.62 KJ/mol and 45.29 ± 2.89 KJ/mol,respectively. Feasible conditions were obtained as follows:operating temperature = 20℃, acetaldehyde: 2,3-butanediol = 0.5:1 (w/w), cyclohexane: fermentation broth = 0.5:1 (w/w), catalyst amount = 100 g/L, stirring rate = 500 rpm and three-stage counter-current extraction method was used. Under these conditions, the total yield rate of 2,3-butanediol from fermentation broth was over 90% and the mass fraction of 2,3-butanediol in the final product reached 99%.
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Yanyang Wu,Yanjun Li,Jiawen Zhu,Jiaxian Liu 한국화학공학회 2013 Korean Journal of Chemical Engineering Vol.30 No.1
An effective process was developed to separate 2,3-butanediol (2,3-BD) from fermentation broth (FB)by reactive-extraction. Propionaldehyde (PRA) was used as reactant and reaction product 2-ethyl-4,5-dimethyl-1,3-dioxolane (EDD) acted as extractant. HCl was selected as catalyst. Appropriate conditions were obtained by experiment as follows: 10 oC, CHCl=0.2mol·L−1, two-stage cross-current extraction, reactant volume ratio (VPRA : VFB) for first stage and second stage is 0.10 and 0.05, respectively. The yield rate of 2,3-butanediol for the whole process can reach 90%w/w, and 2,3-butanediol in the final product can be more than 99% w/w. The novel process required less solution and especially had advantages in treating dilute fermentation broth. Furthermore, equilibrium and kinetic study were investigated on the reaction of propionaldehyde and 2,3-butanediol to provide basic data for process development. The results reveal that reaction enthalpy and activation energy of the reaction were −21.84±2.38 KJ·mol−1 and 51.97±2.84 KJ·mol−1, respectively. Kinetics was well described by pseudo-homogeneous model.
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Reactive extraction of 2,3-butanediol from fermentation broth
Yanyang Wu,Yanjun Li,Jiawen Zhu,Jiaxian Liu 한국화학공학회 2013 Korean Journal of Chemical Engineering Vol.30 No.1
Biochemical 2,3-butanediol is a renewable material, but the lack of an effective separation process limits its industrial application. We developed an effective separation process to recover 2,3-butanediol from fermentation broth by reactive-extraction with ion-exchange resin HZ732 as catalyst. n-Butylaldehyde was used as both reactant and extractant. Feasible operation conditions were obtained as follows: room temperature, Ccat=200 g·L−1, three-stage cross-current extraction, with reactant ratio (VButylaldehyde : Vfermentation broth) 0.05 for each stage. Reactive-extraction can recover over 98% of 2,3-butanediol in the form of 2-propyl-4,5-dimethyl-1,3-dioxolane from fermentation broth. Then 2,3-butanediol was obtained by hydrolyzing 2-propyl-4,5-dimethyl-1,3-dioxolane and purified by vacuum distillation. The total yield rate of 2,3-butanediol through the process was over 94% and purity of final product reached 99%.
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Crystallization and melting behavior of polypropylene in b-PP/polyamide 6 blends containing PP-g-MA
Zhidan Lin,Zixian Guan,Baofeng Xu,Chao Chen,Guangheng Guo,Jiaxian Zhou,Jiaming Xian,Lin Cao,Yueliang Wang,Mingqing Li,Wei Li 한국공업화학회 2013 Journal of Industrial and Engineering Chemistry Vol.19 No.2
In this research, we used a twin-screw extruder to melt and blend PP-g-MA compatibilizer with bpolypropylene (PP)/polyamide 6 (PA6). The influences of the PA6 and PP-g-MA contents in PP/PA6 blends on crystallization and melting behavior of PP phase and morphology were investigated. The results showed that, when PP-g-MA copolymer was added to the b form of nucleated PP/PA6 blends, the anhydride groups in PP-g-MA and PA6 terminal amine groups react to form PP-g-PA graft copolymer in a two-phase interface. This reduces the interfacial tension, improves the interfacial adhesion, and reduces the size of PA6 domains in the blend. The generated PP-g-PA graft copolymer wrapped PA6 phase and buried the anhydride groups of PP-g-MA. When the proportion of PP-g-MA and PA6 was between 0.5 and 0.75, there was no longer interfering to the formation of b-crystals in the PP phase. The content of bcrystal of PP phase in blends was found to reach as large as 85.9%.
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