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Lee, Hwack Joo,Kim, Young Heon,Ryu, Hyun,Cho, Yang-Koo,Nahm, Sahn Korean Society of Microscopy 2017 Applied microscopy Vol.47 No.3
A homogeneous $KNbO_3$ (KN) phase was formed by sintering at $1,040^{\circ}C$ for 1 hour, without formation of the $K_2O$-deficient secondary phase even though suffering the minor loss of $K_2O$. KN liquid phase was formed during sintering and abnormal grain growth occurred in this specimen. The detailed microstructural observations on KN during sintering were carried out using high resolution transmission electron microscopy. The ledged structures were found at the KN grain boundary and the abnormal grain growth was performed by the lateral migration of these ledges in the presence of the liquid phase. The liquid pockets were found in the KN grains. They have various external shapes mainly due to the kinetic factors. They have atomically flat interfaces with some ledges with one atomic height. The slight deficient $K_2O$ by evaporation might somewhat reduce the melting point of KN from the reported at $1,058^{\circ}C$. The liquid pockets play an important role in supplying the liquid phase during the abnormal grain growth in the sintering process of KN ceramics.
이확주,Lee, Hwack-Joo 한국현미경학회 2004 Applied microscopy Vol.34 No.4
In this review, the kinematical scattering theorems are explained by means of Fourier transformation of the assemblies of atoms. The reciprocal space and the generalized Patterson function are introduced. The scatterings of real monatomic gas or liqiud and the hydrogen atoms are described as examples. 물질을 이루고 있는 원자의 집합체에서 단 한번의 회절이 일어나는 경우의 회절이론의 개발을 소개하였다. Fourier transform으로 이루어지는 역 격자 공간에서의 역격자 공간 분포와 실 공간에서의 패터슨 함수와의 관계를 유도하고 이어 여러 가지 물질을 예로 들어 고찰하였다.
2원계 아공석 Ti-Co, Ti-Fe 합금의 공석반응 온도 아래의 온도에서 초석 ${\alpha}$ 반응
이확주,Lee, Hwack-Joo 한국현미경학회 1994 Applied microscopy Vol.24 No.3
A TEM study on proeutectoid ${\alpha}$ reaction at sub-eutectoid temperatures has been made in hypoeutectoid Ti-3.gw/o Co and Ti-5.2w/o Fe alloys. Widmanstatten ${\alpha}$ plates were formed in both alloys within the ${\beta}$ matrix with some modification of degenerate forms. These degenerate plates were formed by the sympathetic nucleation of ${\alpha}$ plates at ${\alpha}:{\beta}$ interphase boundaries. Three types of sympathetic nucleation, i.e., edge-to-edge, face-to-edge, face-to-face, were found in both alloys. The edge-to-edge sympathetically nucleated crystals formed a low-angle boundary between two crystals. The ${\alpha}:{\beta}$ interphase boundaries were found to be partially coherent interfaces which consist of regularly spaced misfit dislocations. The growth of these interphase boundaries were accomplished by the lateral movement of growth ledges. The intersection points of two ${\alpha}$ plates or the low angle boundaries which had formed by edge-to-edge sympathetic nucleation played a role as the potential sources of growth ledges during the growth of plate. The interfacial structures and the spatial morphologies of the degenerate proeutectoid ${\alpha}$ plates would be expected to influence the nucleation and growth of the succeeding eutectoid decomposition process.
TEM 관련 이론해설 (3): 영상 형성이론과 회절이론
이확주,Lee, Hwack-Joo 한국현미경학회 2003 Applied microscopy Vol.33 No.3
영상이론과 회절 이론을 같은 비중으로 다루고 이들과의 관계를 나타내는 wave optics 이론을 소개하였다. 결맞는 파동 이론과 결 안맞는 파동이론 사이의 차이를 나타내고 Abbe이론과 여러 가지 phase contrast 이론들을 small angle 근사로 접근하였다. 마지막으로 다중 성분 시스템에 대한 파동 광학의 수학적인 방법의 적용을 소개하였다. In this review, theoretical approaches of imaging and diffraction in electron microscopy are introduced which allows the diffraction patterns and images to be treated with equal facility and emphasized the relationships between them. The coherent wave optics, incoherent wave imaging theory were introduced. The idea of Abbe theory was also introduced. Varoius phase contrast theories in small angle approximation were derived including the wave theory on Multi-component system.
TEM 관련 이론해설 (4): 방사선의 종류와 물질에 의한 산란
이확주,Lee, Hwack-Joo 한국현미경학회 2003 Applied microscopy Vol.33 No.4
In this review, the sources and the characteristics of X-rays and electrons and their interactions with matters were described in terms of the atomic scattering factors. The geometrical diffraction conditions were taken into account in terms of Ewald spheres in reciprocal lattice spaces. The effects of the finite size of sources and detectors on diffractions were also considered. 물질의 구조 특성파악에 많이 사용되는 X-선과 전자선에 대한 소스 원을 살펴보고 물질과의 반응을 atomic scattering factor의 항으로 설명하였다. 물질과의 회절을 역 격자 공간에서의 Ewald sphere로 설명하고 유한 크기의 소스 파장과 검출기의 효과도 함께 고려하였다.
TEM 관련 이론해설 (6): 투과전자현미경의 고분해능 영상이론: 결맞음 (1)
이확주,Lee, Hwack-Joo 한국현미경학회 2005 Applied microscopy Vol.35 No.3
고분해능 TEM 영상 이론의 결맞음 조사에서의 결맞음에 관한 개념을 소개하였다. 현미경에서 부분 결맞음 파동으로 인한 transfer function과 envelope의 발생을 설명하고 현미경의 분해능과 관련된 passband와 Scherzer 초점 조건을 소개하였다. In this review, the important ideas of coherence theory are introduced. The transfer function and damping envelopes of the microscope due to temporal and spatial coherence are described. The passbands and the condition of Scherzer focus are also disscussed in associated with the resolution of transmission electron microscope.
이확주,Lee, Hwack-Joo 한국현미경학회 2002 Applied microscopy Vol.32 No.3
TEM 이론의 기초가 되는 델타함수, 콘볼루션 적분, 퓨리에 변환에 관한 개념을 소개하고 이에 대한 응용으로 슬릿함수, 현저한 폭을 갖는 2개의 슬릿, 유한 크기의 파동 train, 좁은 슬릿의 주기적인 배열, 임의의 주기 함수, diffraction grating, 회절 격자, 그리고 gaussian 함수에서의 퓨리에 변환에 관한 수학적인 방법의 적용을 소개하였다. In this review, the fundamental concepts of delta function, convolution integral and Fourier transformation are discussed. The applications of Fourier transformation to slit function, two very narrow slits, two slits of appreciable width, periodic array of narrow slits, arbitary periodic function, diffraction gratings and gaussian functions are also introduced.
TEM 관련 이론해설(7): 투과전자현미경의 고분해능 영상이론: 결맞음 (2)
이확주,Lee, Hwack-Joo 한국현미경학회 2006 Applied microscopy Vol.36 No.1
고분해능 TEM 영상 이론의 결맞음 조산에서의 결맞음에 관한 개념을 소개하였다. 현미경에서 부분 결맞음 파동으로 인한 transfer function과 envelope의 발생을 설명하고 현미경의 분해능과 관련된 passband와 Scherzer 초점 조건을 소개하고 결맞음 특성에 관하여 소개하였다. In this review, the important ideas of coherence theory are introduced. The transfer function and damping envelopes of the microscope due to temporal and spatial coherence are described. The passbands and the condition of Scherzer focus are discussed in associated with the resolution of transmission electron microscope. The characterization of coherence is also described.