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Mauro Banchero,Ratna Dewi Kusumaningtyas,Giuseppe Gozzelino 한국공업화학회 2014 Journal of Industrial and Engineering Chemistry Vol.20 No.6
Process intensification through reactive distillation (RD) could be successfully applied to theesterification of long-chain fatty acids, which is a crucial step in the biodiesel synthesis. Whileprevious literature reports are mainly focused on the esterification of short- tomedium- fatty acids, oleicacid has been chosen as an example of a long chain one and different RD configurations were simulatedand compared. The configuration with top external recycle proved to be the best solution since it allowsthe reaction to be conducted under a large methanol excess, even though the column is fed withstoichiometric reactants.