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Bis(N-Methylphenazinium) Bis(Oxalato)Palladate(Ⅱ)의 결정구조
김세환,남궁해,이현미,Kim, Se Hwan,NamGung, Hae,Lee, Hyeon Mi 대한화학회 1994 대한화학회지 Vol.38 No.11
(N-methylphenazinium) bis(oxalato)palladate(II)$((C_{13}H_{11}N_2)_2[Pd(C_2O_4)_2])$의 착이온 및 결정의 구조는 X-선 회절법으로 연구하였다. 이 결정은 사방정계이고 공간군은 P1 (군번호 = 2)이다. 단위세포 길이는 a = 7.616(8), b = 9.842(3), c = $20.335(7)\AA$, $\alpha$ = 103.53(3), $\beta$ = 90.00(5), $\gamma$ = $112.38(5)^{\circ}이며$, $V = 1363(2){\AA}^3,\;F_w = 672.93,\;D_c = 1.639\;gcm^{-3},\;F(000) = 680.0,\;{\mu} = 7.3\;cm^{-1},\;Z = 2$이다. 회절반점들의 세기는 흑연 단색화 장치가 있는 자동 4축 회절기로 얻었으며 $Mo-K\alpha$ X - 선(${\lambda}$= 0.7107 $\AA)$을 사용하였다. 구조분석은 중금속법으로 풀었으며, 최소자승법으로 정밀화하였고, 최종 신뢰도 값들은 3120개의 회절반점에 대하여 $R = 0.069,\;R_w = 0.050,\;R_{all} = 0.069$ 및 S = 5.45였다. 착이온들은 근본적인 평면구조로써, 이들의 충진구조는 착음이온들을 두개의 양이온들이 거의 평행하게 둘러싸고 있는 삼중체들을 형성하고 있다. 양이온과 음이온들의 이면각들이 각각 6.3(6)과 $57.06(6)^{\circ}$인 삼중체들이 b축을 따라서 배열되어 있으나, 삼중체면의 배향은 두 가지 착음이온의 이면각이 $59.08(9)^{\circ}$을 이루는 방향이다. 삼중체내의 면간거리는 각각 3.328와 3.463 $\AA$이었다. The crystal structure of bis(N-methylphenazinium) bis(oxalato)palladate(II) has been determined by X-ray crystallography. Crystal data: ((C_{13}H_{11}N_2)_2[Pd(C_2O_4)_2]) $M_w$ = 672.93, Triclinic, Space Group P1 (No = 2), a = 7.616(8), b = 9.842(3), c = $20.335(7)\AA$, $\alpha$ = 103.53(3), $\beta$ = 90.00(5), $\gamma$ = $112.38(5)^{\circ}$, Z = 2, $V = 1363(2){\AA}^3\;D_c = 1.639\;gcm^{-3},\;{\mu} = 7.3\;cm^{-1},\;F(000) = 680.0$. The intensity data were collected with $Mo-K\alpha$ radiation (${\lambda}$= 0.7107\;\AA)$ on an automatic four-circle diffractometer with a graphite monochromater. The structure was solved by Patterson method and refined by full matrix least-square methods using Killean & Lawrence weights. The final R and S values were $R = 0.069,\;R_w = 0.050,\;R_{all} = 0.069$ and S = 5.45 for 3120 observed reflections. Both cation and anion complexes are essentially planar and have dihedral angles of 6.3(6) and $57.06(6)^{\circ}$ between their planes. The planar complex anions are sandwiched between slightly bent cations. The interplanar separations of two triads are 3.328 and 3.463 $\AA$, respectively. The triads are stacked along b-axis, but their orientations are different based on dihedral angle $59.08(9)^{\circ}$ of two complex anions.
김세환,이성,Kim, Se-Hwan,Lee, Sung 한국교육녹색환경연구원 2004 교육·녹색환경연구 Vol.4 No.4
The thermal effect of a transparent insulated opake wall with solar energy was investigated theoretically. The heat gain through transparent insulated opake wall was studied for relative simple conditions. The stationary heat transport effect was studied for layer which is built on the opake wall. This study shows that a relative low solar radiation intensity causes a great heat reduction through the transparent insulated opake wall. Because the transparent insulation layer is mostly transparent to solar radiation, it is opaque to heat radiation.
실내환경 복원을 위한 다시점 카메라로 획득된 부분적 3차원 점군의 정합 기법
김세환,우운택,Kim Sehwan,Woo Woontack 대한전자공학회 2005 電子工學會論文誌-CI (Computer and Information) Vol.42 No.3
본 논문에서는 실내환경의 3차원 복원을 위해 다시점 카메라부터 획득된 부분적인 3차원 점군에 대한 정합 기법을 제안한다. 일반적으로, 기존의 정합 방법들은 많은 계산량을 요하며, 정합하는데 많은 시간이 소요된다 또한, 상대적으로 정밀도가 낮은 3차원 점군에 대해서는 정합이 어렵다. 이러한 문제점을 해결하기 위해 투영 기반 정합 방법을 제안한다. 첫 번째, 시간적 특성을 기반으로 변화량이 큰 3차원 점들을 제거하고, 공간적 특성을 이용하여 현재 화소의 주변 3차원 점을 참조하여 빈 영역을 채움으로써 깊이 영상 정제 과정을 수행한다. 두 번째, 연속된 두 장면에서의 3차원 점군을 동일한 영상 평면으로 투영하고, 두 단계 정수 매핑을 적용한 후 수정된 KLT (Kanade-Lucas-Tomasi) 특징 추적기를 사용해 대응점을 찾는다. 그리고 적응적 탐색 영역에 기반하여 거리 오차를 최소화함으로써 정밀한 정합을 수행한다. 마지막으로, 대응되는 점들에 대한 색을 참조하여 최종적인 색을 계산하고, 위의 과정을 연속된 장면에 적용함으로써 실내환경을 복원한다. 제안된 방법은 대응점을 2차원 영상 평면에서 찾음으로써 계산의 복잡도를 줄이며, 3차원 데이터의 정밀도가 낮은 경우에도 정합이 효과적이다. 또한, 다시점 카메라를 이용함으로써 몇 장면에 대한 색과 깊이 영상만으로도 실내환경의 3차원 복원이 가능하다. In this paper, a registration method is presented to register partial 3D point clouds, acquired from a multi-view camera, for 3D reconstruction of an indoor environment. In general, conventional registration methods require a high computational complexity and much time for registration. Moreover, these methods are not robust for 3D point cloud which has comparatively low precision. To overcome these drawbacks, a projection-based registration method is proposed. First, depth images are refined based on temporal property by excluding 3D points with a large variation, and spatial property by filling up holes referring neighboring 3D points. Second, 3D point clouds acquired from two views are projected onto the same image plane, and two-step integer mapping is applied to enable modified KLT (Kanade-Lucas-Tomasi) to find correspondences. Then, fine registration is carried out through minimizing distance errors based on adaptive search range. Finally, we calculate a final color referring colors of corresponding points and reconstruct an indoor environment by applying the above procedure to consecutive scenes. The proposed method not only reduces computational complexity by searching for correspondences on a 2D image plane, but also enables effective registration even for 3D points which have low precision. Furthermore, only a few color and depth images are needed to reconstruct an indoor environment.
합금공구강(STD 11)의 방전가공면 변질층 제거에 관한 연구
김세환,Kim, Sei-Whan 한국금형공학회 2007 한국금형공학회지 Vol.1 No.1
This paper has comparatively analyzed the characteristics of the machined surface of a specimen made by machining Die Steel STD11 and a specimen obtained by W-EDM steel. If a press die is manufactured through W-EDM, products of shapes that cannot easily be made through machining can be manufactured easily. However, the life of the press die is significantly reduced compared with the press die made through machining. This is believed to be caused by the deformed layer that has occurred on the surface of the press die that was made through W-EDM. The roughness of the 2 specimens was measured, and it was learned that the distribution of the roughness of the specimen made through the 1st W-EDM was rough.
$[Ni(C_2N_2H_8)_3]\cdotCr_2O_7$의 결정구조
김세환,김승빈,남궁해,Kim, Se-Hwan,Kim, Seung-Bin,Nam, Gung-Hae 한국결정학회 1996 韓國結晶學會誌 Vol.7 No.1
Tris(ethylenediamine)nickel(II)Dichromate [Ni(C2N2H8)3]·Cr2O7착화합물 및 결정의 구조를 X-선 회절법으로 연구하였다. 이 결정은 단사정계이고, 공간군은 P21/b(군번호=14)이다. 단위세포길이는 a=8.268(2), b=13.865(2), c=14.921(2)Å, γ=102.04(2)°, V=1672.9(5)Å3, Z=4, Dc=1.806 gcm-3, μ=24.05 cm-0.1이다. 회절반점들의 세기는 흑연 단색화 장치가 있는 자동4축 회절기로 얻었으며 Mo-Kα X-선(λ=0.7107Å)을 사용하였다. 구조분석은 중원자법으로 풀었으며, 최소자승법으로 정밀화 하였을 때, 최종 신뢰도 값들은 2248개의 회절반점에 대하여 R=0.045, Rw=0.051, Rall=0.059 및 S=2.171이었다. 니켈 착이온 가운데 하나의 에칠렌디아민 고리중에서 두 개의 탄소원자가 무질서하게 상호교차하는 네 개의 원자로 나타났다. 무질서한 에칠렌디아민의 두가지 고리구조들의 α- 과 β- 각들이나 수소결합들을 고려하였을 때 Ni-착이온의 입체구조는 Λδδδ-와 Λδδλ- 구조들의 무질서배열로 보아진다. The crystal structure Tris(ethylenediamine)nickel(II)Dichromate has been determined by X-ray crystallography. Crystal data: a=8.268(2), b=13.865(2), c=14.921(2)Å, γ=102.04(2)°, V=1672.9(5)Å3, Z=4, Monocline, P21/b (space group No.=14), Dcalc=1.806 gcm-3, μ=24.05 cm-0.1. The intensity data were collected with Mo-Kα radiation(λ=0.7107Å) on an automatic four-circle diffractometer with a graphite monochromator. The structure was solved by Patterson method and refined by full matrix least-square methods using unit weights. The final R and S values were R=0.045, Rw=0.051, Rall=0.059 and S=2.171for 2248 observed reflections. The two carbon atoms of a ring of Ni(en)-ion were split into crossed four atoms. In consideration of α- and β-angles of two rings of a disordered ethylenediamine of Nien3-ion and the hydrogen bonds between Ni(en)3-cation and Cr2O7-anion, the configuration of Ni(en)3-ion is assumed to be disordered with Λδδδ and Λδδλ.
반도체금형에서 부속부품의 재료선정 및 개선과 제작에 관한 연구
김세환,최계광,Kim, Sei-hwan,Choi, Kye-kwang 한국금형공학회 2014 한국금형공학회지 Vol.8 No.1
Alloy tool steel such as SKD11 and SKD61 or high speed tool like SKH51 are used as materials for semiconductor dies. Cavities, curl blocks, pot blocks and housings are made from those materials. To make those parts from alloy tool steel or high speed tool, one utilizes discharge machining, and mechanical machining including machining center, milling, drilling, forming grinding and others. In the process of cutting machining and polishing, the die materials become unsuitable for machining owing to bubbles and foreign substances in them, which hinders production process. Therefore, this study focuses on die material selection criteria, and on analysis and comparison of material characteristics to help companies to solve their problems, make die manufacture less burdensome and extend die life.
김세환,최계광,Kim, Sei-hwan,Choi, Kye-kwang 한국금형공학회 2014 한국금형공학회지 Vol.8 No.1
This study is about 3D design for parts supporting copper pipes of wall-mounted air-conditioners manufactured by company "D" in Japan. Domestic press die manufacturers are obsessed with 2D die design and are afraid of taking risk with developing 3D die design and die manufacture. This hinders paradigm shift. In this study, the strip layout, which was already completed in the previous study, is altered by adding restriking. Based on the modified strip layout, the 3D die design is done in 15 processes.
내통의 플래시 및 충진불량에 대한 해결방법에 관한 연구
김세환,최계광,이춘규,Kim, Sei-hwan,Choi, Kye-kwang,Lee, Choon-kyu 한국금형공학회 2012 한국금형공학회지 Vol.6 No.2
Inner part is used as an insulator in wire fuses. After injection molding, inner part has been showed flashes, filling defects and deformation. After production, operators have to cut off flashes, one by one. this process leads to continuous low productivity and loss of source materials. This study focuses on identifying the causes for flashes, filling defects, clamping force of injectors, mold adhesion, resin of liquidity and others, and on resolving those issues.
김세환,최계광,Kim, Sei-hwan,Choi, Kye-kwang 한국금형공학회 2014 한국금형공학회지 Vol.8 No.1
Even though 3D press die design gains more attention everyday in Korea, there are shortages of infrastructure and proper environments for it. What is most needed is human resources development and 3D die design standardization, on which the pace of 3D die design adoption depends. This study focuses on 3D press die design process by looking into an instance in which 3D die design system had been used to sell dies to a company "S" in Japan.