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김동욱,조옥연,정춘환,Kim, Dong-Uk,Cho, Ok-Yon,Jeong, Chun-Hwan 한국건축역사학회 2005 건축역사연구 Vol.14 No.1
This study is the consideration about Hwaryeong-Jeon that enshrines Joseon Dynasty 22nd king Jeongjo's portrait of a king. Suwon's Hwaryeong-Jeon that accompanied a portrait and performed ritual ceremonies had several formalities and ceremonies which are connected with rituals. therefore, we will try to examine what relation between arrangement of building and plane composition had. And through this, it is thing to observe construction special quality that Hwaryeong-Jeon has. Joseon Dynasty's young-jeon (a hall where the royal portraits are kept) is retaining each other different state according to construction age every moment. Hwaryeong-Jeon among Joseon Dynasty's a hall of royal portraits is the construction form which is equiped well and is known for keeping the form well from the foundation to now And this building is evaluated as the standard form of early part young-jeon building of 19th century. Especially, Hwaryeong-Jeon shows the typical ritual equipments late Joseon Dynasty and at the same time has all kinds of characteristics which only we can find at Hwaryeong-Jeon. Namely, Hwaryeong-Jeon is the building which brings the design concept of the hall of royal portraits to completion as the building which enshrines single portrait of a king. After all, Hwaryeong-Jeon is evaluated as the building which can pass excellent form of late Joseon Dynasty, the hall of royal portraits building just as it is. Therefore, as I study its own style, I expect Joseon Dynasty's mind that enshrined the portrait of a king elaborately to be revealed.
직접 메탄올 연료전지용 나피온 막의 폴리아닐린/Sulfonated Poly(ether sulfone) 다층 자기조립 박막에 의한 표면 개질
옥정림,김동욱,이창진,강영구,Ok, Jeong-Rim,Kim, Dong-Wook,Lee, Chang-Jin,Kang, Yong-Ku 한국전기화학회 2008 한국전기화학회지 Vol.11 No.4
본 연구에서는 나피온 막을 통한 메탄올 투과도를 감소시키기 위하여 양전하를 띠는 polyaniline(PANi)와 음전하를 갖는 sulfonated Poly(ether sulfone)(SPES)으로부터 다층 자기조립 박막법으로 나피온 막의 표면을 개질하였다. PANi과 SPES는 열적 화학적으로 안정하며 매우 강직한 특성을 띄고 있어, 나피온 막 표면에 다층 자기조립 박막 형성시 메탄올 투과도 감소 및 치수 안정성의 향상을 기대할 수 있다. 자외선-가시광선 흡광분석에 의하여 PANi와 SPES의 다층박막의 형성이 균일하게 이루어짐을 확인 하였다. TEM 분석을 통하여 다층 자기조립 박막의 bilayer당 두께가 약 10 nm 정도임을 확인 하였다. 개질된 나피온 막은 순수한 나피온 막에 비하여 15%의 이온전도도 감소가 일어났지만 67%의 높은 메탄올 투과도 감소를 나타내어 2.5배 높은 선택도를 보였다. 5 M 메탄올을 연료로 사용한 연료전지 성능시험에서 개질된 나피온 막은 순수한 나피온 막에 비해 최대 전력 밀도가 $30^{\circ}C$에서는 2.4배 증가, $60^{\circ}C$에서는 1.4배 향상을 나타내었다. In this study, Nafion membrane was modified to prevent methanol crossover by layer-by-layer self assembly using polyaniline (PANi) as a polycation and sulfonated poly(ether sulfone) (SPES) as a polyanion onto the Nafion surface. Since PANi and SPES possess thermal and chemical stability and rigid backbone, their layer-by-layer self-assembled films on the Nafion are expected to reduce methanol permeability and to increase mechanical stability. UV-Vis absorption spectroscopy verified a linear build-up of the multilayers of PANi and SPES. We found that the thickness per bilayer was about 10 nm by TEM measurement. Although modified Nafion membrane exhibited 15% decrease of proton conductivity, it reduceded 67% of methanol permeability compared to that of the pristine Nafion membrane, resulting in 2.5 times larger selectivity. At the performance test of the fuel cell using 5M methanol as a fuel, the modified Nafion membrane showed 2.4 times higher maximum power density at $30^{\circ}C$ and 1.4 times larger at $60^{\circ}C$ than the pristine Nafion.