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알킬이미다졸린과 지방산 카르바미드를 이용한 내구성 유연제의 제조에 관한 연구
정충호,박홍수,김영근 ( Choong Ho Jung,Hong Soo Park,Young Keun Kim ) 한국공업화학회 1993 공업화학 Vol.4 No.1
Dodecanoic acid와 tetraethylenepentamine을 반응시켜서 1, 2-disubstituted imidazoline을 얻었고, 이것을 양이온화시켜 유화형 1, 2-disubstituted imidazolinium salt를 합성하였다. 또한 docosanoic acid와 hydroxyethylethylenediamine을 반응시켜 중간생성물인 2-docosamido-2`-docosanoyloxydiethylamine을 얻었고, 다시 우레아와 반응시켜서 지방산 카르바미드를 얻었다. 이것을 역시 양이온화시켜 유화형 지방산카르바미드염을 합성하였다. 합성된 각종 염들을 블렌딩시켜 유연제를 제조한 후, 아크릴 섬유에 유연처리를 하여 유연성, 평활성 및 대전방지성을 측정한 결과, 유연성과 평활성이 양호하였고 약간의 대전방지성도 보유하였다. 또한 강연도시험과 pH변화에 따른 촉감의 내세탁성 시험결과를 통하여 제조된 유연제가 내구성 유연제임을 입증하였으며, SEM으로 유연처리된 아크릴 섬유의 표면구조를 관찰하였다. Some emulsified 1, 2-disubstituted imidazolinium salts were synthesized by quaternization of 1, 2-disubstituted imidazoline which had been prepared by the reaction of dodecanoic acid with tetraethylenepentamine. 2-Docosamido-2`-docosanoyloxydiethylamine was prepared by the reaction of docosanoic acid with hydroxylethylethylenediamine. Then, some emulsified fatty carbamide salts were also synthesized by quaternization of fatty carbamide which had been prepared by the reaction of urea with the 2-docosamido-2`-docosanoyloxydiethylamine. Some softners were prepared by blending of these salts mentioned above. These softners were treated on acrylic fiber, then several properties were measured. As the results, softening and lubricating properties are good, and a little antistatic property was observed. The synthesized softners were also proved as a durable softner by means of the several experiments : bending resistance test and measurements of feeling change with washing according to the pH changes. The surface structure of acrylic fibers treated with the softner were characterized by SEM.
카프로락톤기 함유 80퍼센트 고형분인 아크릴수지와 HMDI-Trimer에 의한 하이솔리드 도료의 도막물성
정충호,김승진,박홍수,조혜진,심일우,김성길 한국응용과학기술학회 2006 한국응용과학기술학회지 Vol.23 No.2
The high-solid coatings were prepared by blending the synthesized acrylic resin in the previous paper, and hexamethylene diisocyanate-trimer and curing it at room temperature. The characterization of the films of the prepared coatings was performed. The 60° specular gloss, impact resistance, cross-hatch adhesion, and heat resistance of the films proved to be good, and the pencil hardness, drying time, and pot-life proved to be slightly poor. From a viscoelastic measurement using a rigid-body pendulum, curing was accelerated with the Tg value.
I카프로락톤기 함유 90% 고형분인 아크릴수지의하이솔리드 도료에의 적용
양인모*김승진*김영근*정충호**박홍수 한국응용과학기술학회 2007 한국응용과학기술학회지 Vol.24 No.2
In order to prepare high-solid coatings, acrylic resins, HSCs [poly(EA/EMA/2-HEMA/CLA)] that contain 90% solid, were synthesized by copolymerization of ethyl acrylate (EA), ethyl methacrylate (EMA), 2-hydroxyethyl methacrylate (2-HEMA) and caprolactone acrylate (CLA). The high-solid coatings named as CHSCs (HSCs/HDI-trimer) were prepared by the curing reaction between the acrylic resins containing 90% solid contents and the isocyanates (HDI-trimer) curing agent room temperature. The curing behavior and various properties were examined on the film coated with the both high-solid coatings. The glass transition temperatures (Tg) of CHSCs increased proportionally with increasing the predicted Tg value by Fox equation, and had nothing to do with the solid contents. The prepared film showed good properties for 60° specular gloss, impact resistance, cross-hatch adhesion and heat resistance, and bad properties for pencil hardness, drying time, and pot-life. Among the film properties, the heat resistance was very excellent and could be explained by the introduction of functional monomers of CLA.
피로포스포릭 락톤 변성폴리에스테르를 함유한 폴리우레탄 난연도료의 물성 및 난연효과
정충호(Choong Ho Jung),최용호(Yong Ho Choi),박홍수(Hong Soo Park) 한국유화학회 2000 한국응용과학기술학회지 Vol.17 No.3
Pyrophosphoric lactone modified polyester(PATT) that contains two phosphorous functional groups in one unit base resin structure was synthesized to prepare a non-toxic reactive flame retardant coatings. Then the PATT was cured at room temperature with isocyanate, Desmodur IL, to get a two-component polyurethane flame retardant coatings(PIPUC). Comparing the physical properties of the films of PIPUC with the film of non-flame retardant coatings, there was no degradation observed in physical properties by the introduction of a flame-retarding component into the resin. We found that the char lengths measured by 45˚Meckel burner method were 3.1~4.4㎝ and LOI values recorded 27~30%. These results indicate that the coatings prepared in this study is good flame retardant one. The surface structure of coatings investigated with SEM does not show any defects and phase separation. Keywords : non-toxicity, reactive type, polyurethane coatings, flame retardancy.
정충호 ( Choong Ho Jung ),강태희 ( Tae Hee Kang ) 한국유화학회 2010 한국응용과학기술학회지 Vol.27 No.4
In this research, we were prepared the glazed ceramic samples by the change of the pigment content and investigated to reveal the standardized color. The chemical composition of the pigment was analyzed using a ICP-OES. XRF mapping and UV-Vis spectroscopy were used to evaluate the color property and surface homogeneity. The color development was observed as a result of analyzing the pigment content and change of the color. The pigment content and the spectral reflection showed the relation of the inverse proportion and the standardized color which could be revealed through analysis data.
정충호 ( Jung-choong Ho ),김종문 ( Chong-mun Kim ),김기수 ( Ki-su Kim ),최윤수 ( Yun-soo Choi ) 한국지리정보학회 2019 한국지리정보학회지 Vol.22 No.2
1961년 공공측량 제도가 도입되었을 때는 사회기반시설 건설공사와 같은 대규모 측량성과가 주를 이루었지만, 환경변화에 따라 소규모 지하시설물 위주의 측량성과가 대부분을 차지하고 있다. 지하시설물의 측량방법은 관로 매설 후 되메우기 전 실측하는 방법과 되메우기 후 탐사를 이용하는 방법이 있으며, 각각의 장단점이 존재한다. 그러나 탐사를 통해 관로가 관측되지 않는 불탐구간의 발생으로 지하시설물의 위치정확도 확보가 어려워지자 2017년 성과심사 규정을 개정하여 ‘지하시설물도 작성시기’ 항목을 추가하였고 실측을 중심으로 심사하게 된다. 그러나 현장에서는 이와 관련하여 탐사의 장점과 실측의 한계에 대한 의견이 지속적으로 제기되어 왔다. 이에 본 연구에서는 공공측량 제도의 배경과 목적을 고려하여 지하시설물 측량이 공공측량에서 차지하는 비중을 확인하고, 공공측량 시행자 및 수행자를 대상으로 설문조사를 수행, 분석하여 현장 의견을 종합한 개선안을 제시하였다. When the public surveying system was introduced in 1961, large scale surveying performances, such as infrastructure construction work, were dominant. However, due to changes in the environment, most of the current surveying performances focused on small scale underground facilities. The method of surveying underground facilities is as follows: “method of measurement before refilling after burying the pipeline” and “method of using exploration after refilling.” There are advantages and disadvantages to each method. It became difficult to obtain the accuracy of the location of the underground facilities due to the fact that there were sections of the pipeline that had not been observed through exploration. Therefore, the 2017 performance evaluation regulations were revised. The revision included the addition of the “Underground Facilities Creation Period,” a system that allows for surveys to be evaluated based on actual measurements. However, in this particular field, concerns about the advantages of exploration and the purpose of this study was to investigate the background and purpose of the limitations of the survey have been continuously raised. The purpose of this study was to investigate the background and purpose of the public surveying system and to identify the proportion of underground facilities surveying in comparison to public surveying. This study conducted surveys on the implementers of public surveying and those who did the actual surveying. The researcher has summarized the improvements that incorporate the analysis results and the field comments in the revised performance evaluation regulations in 2017.
정충호 ( Choong Ho Jung ),김성례 ( Sung Rae Kim ),박형진 ( Hyong Jin Park ),김명수 ( Myung Soo Kim ),박홍수 ( Hong Soo Park ),박신자 ( Shin Ja Park ) 한국유화학회 2002 한국응용과학기술학회지 Vol.19 No.4
N/A Self-diffusion coefficients of colloidal association structures in the aqueous solutions of anionic ammonium dodecyl sulfate (ADS) and cationic octadecyltrimethylammonium chloride (OTAC) surfactants were measured by pulsed-gradient spin echo NMR. The results were interpreted on the basis of the ADS/OTAC/water phase diagram. Crossing the phase boundaries, significant changes in self diffusion coefficients were observed and well correlated to the phase diagram. For the micelles their apparent radii were obtained from Stokes-Einstein equation. Their values were 15 for the ADS micelles and 54Å for the OTAC micelles, respectively. For vesicles which were formed spontaneously at different relative amounts of the surfactants and total surfactant concentrations, the radius was measured as 50 to 200 nm. This result is in fair agreement with those by TEM and light scattering.
지방산 폴리아미드 및 알킬이미다졸린을 이용한 나일론 섬유용 내구성 유연제의 제조
정충호 ( Choong Ho Jung ),김성례 ( Sung Rae Kim ),박형진 ( Hyong Jin Park ),함현식 ( Hyun Sik Hahm ),김태옥 ( Tae Ok Kim ),박홍수 ( Hong Soo Park ) 한국유화학회 2002 한국응용과학기술학회지 Vol.19 No.4
N/A Fatty polyamide that gives softness, lubrication and bulky property and alkyl imidazoline that gives durable softness and antistatic property were synthesized. then, an O/W-type durable softener (DSN) was prepared by the emulsion of the synthesized fatty polyamide and alkyl imidazoline. Emulsion stability of the DSN was good, and the mixed HLB value was 11.2. From the measurement of softness, lubrication, antistatic property, bending resistance, and color fastness, it was proved that the prepared DSN was a good durable softener for nylon.