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(Allyloxy)methyl-Crown Ether를 이용한 액체막계에서의 Pd(Ⅱ) 및 Pb(Ⅱ)의 분리
이용구,조현성,김태순,이동구,김응태,조문환,이영길,채영복,Lee, Yong Gu,Cho, Hyun Sung,Kim, Tae Soon,Lee, Dong Koo,Kim, Eung Tae,Cho, Moon Hwan,Lee, Young K.,Chae, Young Bok 대한화학회 1997 대한화학회지 Vol.41 No.9
(Allyloxy)methyl-Crown Ethers have been used as metal cation carriers in a bulk liquid membrane system. Competitive transports by the AMDT18C6 and the AM18C6 are selective for Pd(Ⅱ) ion and Pb(Ⅱ) ion over other transition metal cations respectively. Studies of complexations of (Allyloxy)methyl-Crown Ethers with metal cations have been carried out by titration calorimetry and potentiometry. (Allyloxy)methyl-Crown Ether를 액체막계에서 금속이온의 운반체로 사용하였다. 운반체로 사용한 AMDT18C6는 경쟁이동반응에서 Pd(II)를 선택적으로 분리하였으며 AM18C6는 Pb(II)의 선택성이 있었다. 거대고리리간드와 금속이온과의 착물형성에 관한 연구는 전위차법과 용액열량계법을 이용하였다.
이용구,박재환,최영진,박재관,Lee, Yong-Koo,Park, Jae-Hwan,Choi, Young-Jin,Park, Jae-Gwan 한국세라믹학회 2010 한국세라믹학회지 Vol.47 No.6
We synthesized ZnO nanowires patterned on Si substrate and investigated the field emission properties of the nanowires. Firstly, Au catalyst layers were fabricated on Si substrate by photo-lithography and lift-off process. The diameter of Au pattern was $50\;{\mu}m$ and the pattern was arrayed as $4{\times}4$. ZnO nanowires were grown on the Au catalyst pattern by the aid of Au liquid phase. The orientation of the ZnO nanowires was vertical on the whole. Sufficient brightness was obtained when the electric field was $5.4\;V/{\mu}m$ and the emission current was $5\;mA/cm^2$. The threshold electric field was $5.4\;V/{\mu}m$ in the $4{\times}4$ array of ZnO nanowires, which is quite lower than that of the nanowires grown on the flat Si substrate. The lower threshold electric field of the patterned ZnO nanowires could be attributed to their vertical orientation of the ZnO nanowires.
Helicobacter pylori 제균 후 위축위염과 장상피화생의 변화
이용구 ( Yong Gu Lee ),전용철 ( Yong Cheol Jeon ),구태연 ( Tai Yeon Koo ),조현석 ( Hyun Seok Cho ),변태준 ( Tae Jun Byun ),김태엽 ( Tae Yeob Kim ),이항락 ( Hang Lak Lee ),은창수 ( Chang Soo Eun ),이오영 ( Oh Young Lee ),한동수 ( D 대한소화기학회 2007 대한소화기학회지 Vol.50 No.5
목적: Helicobacter pylori 감염이 장기간 지속될 경우 위축위염과 장상피화생을 초래하여 위암 발생 위험이 증가한다. 그러나 H. pylori를 제균하는 것이 위축변화나 장상피화생을 회복시킬 수 있을지는 아직 이견이 많다. 따라서 저자들은 H. pylori 제균 후에 위축과 장상피화생의 변화 여부를 조사하였다. 대상 및 방법: 2001년 3월부터 2006년 4월까지 방문한 107명의 H. pylori 제균에 성공한 환자들을 대상으로 하였다. 전정부 조직검사를 통해 H. pylori 감염 여부를 판단하였으며 동시에 위축변화와 장상피화생의 정도를 updated Sydney System에 따라 점수화하였다. 전정부 조직검사는 제균 후 일정기간 후에 위내시경검사를 통해 재시행하였고, H. pylori 제균 여부도 조직검사로 확인하였다. 결과: 대상환자의 평균 연령은 55.3±11.3세였으며, 평균 추적기간은 28.7±13.9개월이었다. 내시경 진단은 위궤양, 십이지장궤양, 비궤양 전정부위염의 3가지로 구분하였다. 위축변화는 누락된 자료를 제외한 91명 중 41명에서 관찰되었고, 평균 점수는 0.73±0.92였다. 추적한 위축변화 점수는 0.38±0.70로 제균 후 회복되었다(p=0.025). 그러나 107명 중 49명에서 관찰된 장상피화생은 다소 호전되어 보였으나 통계적인 의미는 없었다. 새로이 발생한 위축변화와 장상피화생이 관찰되었으며 그 평균 점수는 제균 전 위축변화나 장상피화생이 있는 환자에서의 평균보다 낮았으나 통계적인 의미는 없었다. 결론: H. pylori 제균 후에 위축변화는 호전되지만 장상피화생은 호전 정도가 미약하여 호전을 확인하기 위해서는 더 오랜기간 관찰이 필요할 것이다. H. pylori 제균과 위 점막의 위축변화 및 장상피화생 사이의 관계를 확립하기 위해서는 추후 더 큰 규모의 대조군 연구가 필요할 것으로 생각한다. Background/Aims: Long-term Helicobater pylori infection results in atrophic gastritis and intestinal metaplasia, and increases the risk of gastric cancer. However, it is still controversial that eradication of H. pylori improves atrophy or metaplasia. Therefore, we investigated histological changes after the H. pylori eradication in patients with atrophy or metaplasia. Methods: One hundred seven patients who received successful eradication of H. pylori infection in Hanyang University, Guri Hospital from March 2001 to April 2006, were enrolled. Antral biopsy was taken before the eradication to confirm the H. pylori infection and grade of atrophy or metaplasia by updated Sydney System. After a certain period of time, antral biopsy was repeatedly taken to confirm the eradication and investigate histological changes of atrophy or metaplasia. Results: Mean age of the patients was 55.3±11.3, and average follow-up period was 28.7±13.9 months. Endoscopic diagnosis included gastric ulcer, duodenal ulcer, non-ulcer antral gastritis. Atrophy was observed in 41 of 91 and their average score was 0.73±0.92. After the eradication of H. pylori, atrophy was improved (0.38±0.70, p=0.025). However, metaplasia which was observed in 49 of 107, did not significantly improve during the follow-up period. Newly developed atrophy (7 of 38) or metaplasia (18 of 49) was observed in patients who without atrophy or metaplasia initially. Their average scores were slightly lower than those of cases with pre-existing atrophy or metaplasia without statistical significance. Conclusions: After the eradication of H. pylori infection, atrophic gastritis may be improved, but change of intestinal metaplasia is milder and may take longer duration for improvement. (Korean J Gastroenterol 2007;50:299-305)
X형 배근을 적용한 PC기둥-거더 접합부의 구조적 성능에 관한 실험적 연구
이용구(Lee Yong-Koo),홍갑표(Hong Kap-Pyo),이성수(Lee Seung-Su),전호민(Chun Ho-Min),조광수(Cho Kwang-Su),권윤한(Kwon Yun-Han) 대한건축학회 2009 대한건축학회 학술발표대회 논문집 - 계획계/구조계 Vol.29 No.1(구조계)
In the long-span sub-micro vibration control structures, one of the essential factor together with vibration control comply a term of works. therefore applying precast concrete is a point of the present time when we consider to reduction of a term of works. we must devise other special floor system, if it go over the maximum manufactured precast concrete member size. The purpose of this experimental study is to examine the structural properties of X-braced PC column-girder joint in long span sub-micro vibration control structure system of length over 17 meter. The test result showed that X-brace was appeared stress concentration and each point strains of reinforcement bar appeared load-strain curve.
(Allyloxy)methyl-Crown Ether를 이용한 액체막계에서의 Pd(Ⅱ) 및 Pd(Ⅱ)의 분리
이용구(Yong Gu Lee),조현성(Hyun Sung Cho),김태순(Tae Soon Kim),이동구(Dong Koo Lee),김응태 외 3인(Eung Tae Kim 외 3인) 강원대학교 기초과학연구소 1997 기초과학연구 Vol.8 No.-
(Allyloxy)methyl-Crown Ether를 액체막계에서 금속이온의 운반체로 사용하였다. 운반체로 사용한 AMDT18C6는 경쟁이동반응에서 Pd(Ⅱ)를 선택적으로 분리하였으며 AM18C6는 Pb(Ⅱ)의 선택성이 있었다. 거대고리리간드와 금속이온과의 착물형성에 관한 연구는 전위차법과 용액열량계법을 이용하였다. (Allyloxy)methyl-Crown Ethers have been used as metal cation carriers in a bulk liquid membrane system. Competitive transports by the AMDT18C6 and the AM18C6 are selective for Pd(Ⅱ) ion and Pb(Ⅱ) ion over other transition metal cations respectively. Studies of complexations of (Allyloxy) methyl-Crown Ethers with metal cations have been carried out by titration calorimetry and potentiometry
수용액 분사에 의한 아이스 슬러리의 제조에 관한 실험적 연구
이용구(Yong-Koo Lee),오철(Cheol Oh) 한국항해항만학회 2010 한국항해항만학회지 Vol.34 No.1
아이스슬러리의 생성을 위하여 냉각평판에 작동수를 분사하는 실험을 수행하여 그에 대한 영향에 대하여 영향을 평가하였다. 실험에 사용된 에틸렌글리콜 수용액은 1O~20wt%의 수용액을 사용하였다. 실험장치는 슬러리아이스 저장탱크, 브라인 탱크, 브라인 순환장치, 유량계 및 온도기록계로 구성되어 있다. 실험조건은 평균유속 1.0~2.0m/s , 냉각온도 -17~-10'C의 조건 하에 실험을 수행하였다. Thís study is experimented to observe an influence of experimental conditions on production characteristics of slurry ice by injection operating water to cooling plate. And at thís experiment ít used ethylene glycol-water solution and the concentration is 10 to 20wt%. The experimental apparatus was constructed of ethylene glycol-water solution and slurry ice storage tank, brine tank, pumps for ethylene glycol-water solution and brine circulating, a mass flow-meter, data logger for fluid temperature measuring and a vertical circular tube with single copper plate as test section The experiments were carried out under various conditions, with mean velocity of fluid at the entry ranging from 1.0 to 2.0m/s and the cooling temperature of -17'C to -10'C.
임종엽,이용구,박종범,김민영,양계준,임동건,Lim, Jong-Youb,Lee, Yong-Koo,Park, Jong-Bum,Kim, Min-Young,Yang, Kea-Joon,Lim, Dong-Gun 한국전기전자재료학회 2011 전기전자재료학회논문지 Vol.24 No.9
$Cu(In_{1-x},Ga_x)Se_2$ thin films have been considered as an effective absorber material for high efficient solar cells. In this paper, the CIGS thin films with varied Ga content were prepared using a co-evaporation process of three stage. We carry out structure and electrical optical property on the thin film in varied Ga content. CIGS thin films have been characterized by X-ray diffraction(XRD), scanning electron microscopy(SEM), energy-dispersive spectroscopy(EDS), four-point probe measurement, and the Hall measurement. To optimize Ga contents, Ga/(In+Ga) ratio were changed from 0.13 to 0.72. At this time the carrier concentrations were varied from $1.22{\times}10^{11}\;cm^{-3}$ to $5.07{\times}10^{16}\;cm^{-3}$, and electrical resistivity were varied from $1.11{\times}10^0\;{\Omega}-cm$ to $1.08{\times}10^2\;{\Omega}-cm$. A strong <220/204> orientation and a lager grain size were obtained at a Ga/(In+Ga) of 0.3. We were able to achieve conversion efficiency as high as 15.95% with a Ga/(In+Ga) of 0.3.