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SHS 공정에 의해 제조된 Mo<sub>x</sub>W<sub>1-x</sub>Si<sub>2</sub> 발열체의 열화메커니즘
이동원,이상헌,김용남,이성철,구상모,오종민,Lee, Dong-Won,Lee, Sang-Hun,Kim, Yong-Nam,Lee, Sung-Chul,Koo, Sang-Mo,Oh, Jong-Min 한국전기전자재료학회 2017 전기전자재료학회논문지 Vol.30 No.10
The degradation mechanism of $Mo_xW_{1-x}Si_2$ ultrahigh-temperature heating elements fabricated by self-propagating high-temperature synthesiswas investigated. The $Mo_xW_{1-x}Si_2$ specimens (with and without post-annealing) were subjected to ADTs (accelerated degradation tests) at temperatures up to $1,700^{\circ}C$ at heating rates of 3, 4, 5, 7, and $14^{\circ}C/min$. The surface loads of all the specimen heaters were increased with the increase in the target temperature. For the $Mo_xW_{1-x}Si_2$ specimens without annealing, many pores and secondary-phase particles were observed in the microstructure; the surface load increased to $23.9W/cm^2$ at $1,700^{\circ}C$, while the bending strength drastically reduced to 242 MPa. In contrast, the $Mo_xW_{1-x}Si_2$ specimens after post-annealing retained $single-Mo_xW_{1-x}Si_2$ phases and showed superior durability after the ADT. Consequently, it is thought that the formation of microcracks and coarse secondary phases during the ADT are the main causes for the degraded performance of the $Mo_xW_{1-x}Si_2$ heating elements without post-annealing.
탄탈륨 산화물의 마그네슘 가스환원에 의한 탄탈륨 금속분말 제조
이동원,Lee, Dong-Won 한국분말야금학회 2018 한국분말재료학회지 (KPMI) Vol.25 No.5
Metallic tantalum powder is manufactured by reducing tantalum oxide ($Ta_2O_5$) with magnesium gas at 1,073-1,223 K in a reactor under argon gas. The high thermodynamic stability of magnesium oxide makes the reduction reaction from tantalum oxide into tantalum powder possible. The microstructure after the reduction reaction has the form of a mixture of tantalum and magnesium oxide, and the latter could be entirely eliminated by dissolving in weak hydrochloric acid. The powder size in SEM microstructure for the tantalum powder increases after acid leaching in the range of 50-300 nm, and its internal crystallite sizes are observed to be 11.5 to 24.7 nm with increasing reduction temperatures. Moreover, the optimized reduction temperature is found to be 1,173 K as the minimum oxygen concentration is approximately 1.3 wt.%.
마그네슘환원에 의한 C/N 조성제어 초미립 TiC<sub>x</sub>N<sub>y</sub> 분말 합성
이동원,김병기,윤중열,유지훈,김용진,Lee, Dong-Won,Kim, Byoung-Kee,Yun, Jung-Yeul,Yu, Ji-Hoon,Kim, Yong-Jin 한국분말야금학회 2010 한국분말재료학회지 (KPMI) Vol.17 No.2
The ultrafine titanium carbonitride ($TiC_xN_y$) particles below 100 nm in mean size, including various carbon and nitrogen contents (x=0.55~0.9, y=0.1~0.5), were successfully synthesized by new Mg-thermal reduction process. Nanostructured sub-stoichiometric titanium carbide ($TiC_x$) particles were initially produced by the magnesium reduction of gaseous $TiCl_4+x/2C_2Cl_4$ at $890^{\circ}C$ and post heat treatments in vacuum were performed for 2 hrs to remove residual magnesium and magnesium chloride mixed with $TiC_x$. Finally, well C/N-controled $TiC_xN_y$ phases were successfully produced by nitrification heat treatment under normal $N_2$ gas atmosphere at $1150^{\circ}C$ for 2 hrs. The values of purity, mean particle size and oxygen content of produced particles were about 99.3%, 100 nm and 0.2 wt.%, respectively.
이동원,박근태,임태수,이혜문,유지훈,Lee, Dong-Won,Park, Geun-Tae,Lim, Tae-Soo,Lee, Hye-Moon,Yu, Ji-Hun 한국분말야금학회 2011 한국분말재료학회지 (KPMI) Vol.18 No.4
Zr-Ti alloy powders were successfully synthesized by magnesium thermal reduction of metal chlorides. The evaporated and mixed gasses of $ZrCl_4+TiCl_4$ were injected to liquid magnesium and the chloride components were reduced by magnesium leading to the formation of $MgCl_2$. The released Zr and Ti atoms were then condensed to particle forms inside the mixture of liquid magnesium and magnesium chloride, which could be dissolved fully in post process by 1~5% HCl solution at room temperature. By the fraction-control of individually injected $ZrCl_4$ and $TiCl_4$ gasses, the final compositions of produced alloy powders were changed in the ranges of Zr-0 wt.%~20 wt.%Ti and their purity and particle size were about 99.4% and the level of several micrometers, respectively.
마그네슘의 금속염화물 환원에 의한 초미립 TiCN 분말합성
이동원,김진천,김용진,김병기,Lee, Dong-Won,Kim, Jin-Chun,Kim, Yong-Jin,Kim, Byoung-Kee 한국분말야금학회 2009 한국분말재료학회지 (KPMI) Vol.16 No.2
The ultrafine titanium carbonitride particles ($TiC_{0.7}N_{0.3}$) below 100nm in mean size were successfully synthesized by Mg-thermal reduction process. The nanostructured sub-stoichiometric titanium carbide ($TiC_{0.7}$) particles were produced by the magnesium reduction at 1123K of gaseous $TiC_{l4}+xC_2Cl_4$ and the heat treatments in vacuum were performed for five hours to remove residual magnesium and magnesium chloride mixed with $TiC_{0.7}$. And final $TiC_{0.7}N_{0.3}$ phase was obtained by nitrification under normal $N_2$ gas at 1373K for 2 hrs. The purity of produced $TiC_{0.7}N_{0.3}$ particles was above 99.3% and the oxygen contents below 0.2 wt%. We investigated in particular the effects of the temperatures in vacuum treatment on the particle refinement of final product.
이동원,이양,정영우,Lee, Dong Won,Lee, Yang,Chung, Young Woo 영남수학회 2014 East Asian mathematical journal Vol.30 No.4
We can easily see the 'cycloid slide' in the many mathematics and science museums. The educational materials, however, do not give us any mathematical principle. For this reason, we, in this thesis, first study the brachistochrone problem in the history of mathematics, and suggest a method of how to teach the principle using 'the dynamic geometry software GSP5' in order to help students understand the idea that the cycloid is the brachistochrone. Secondly, we examine the origin of the calculus of variations and apply it to prove the brachistochrone problem in order to build up the teachers' background knowledge. This allows us to increase the worth of history of mathematics and recognize how useful the learning is which uses technological tools or materials, and we can expect that the learning which makes use of cycloid slide will be meaningful.
이동원,Hyun Kyu Jeong,박정용,Jong Hyuk Lee,Son Jeong Wang,Yong Hwan Jeong,Young Duk Bae,Bong Guen Hong 한국물리학회 2007 THE JOURNAL OF THE KOREAN PHYSICAL SOCIETY Vol.51 No.3
In order to investigate the manufacturing and qualification methods for the first wall (FW) of the International Thermonuclear Experimental Reactor (ITER), we fabricated several mock-ups with various shapes through the hot isostatic pressing (HIP) bonding method for joining the Cu-alloy with Be armor and the Cu-alloy with stainless steel (SS). Non-destructive test (NDT) methods currently being developed for the ITER FW were applied to these mock-ups to find the defects. Ultrasonic test (UT) showed that a probe of 10 MHz and 0.25 inch in diameter could detect defects up to 3 mm in diameter. The eddy current test (ECT) for the SS tube was simulated with a numerical code and showed the feasibility of detecting defects in the SS tube. Thermography was simulated with a numerical code, CFX-10, and preliminary tests were performed. Also, a high heat flux (HHF) test was performed up to 1000 cycles at 5.0 MW/m2 for the Cu/SS mock-up in Japan (JEBIS, JAEA Electron Beam Irradiation Stand), and it is being prepared for the Be/Cu mock-up in Russia. .