강가공된 순수 Cu의 미세조직과 기계적 특성 평가

송국현,손현택,김대근,김한솔,김원용,Song, Kuk-Hyun,Son, Hyun-Taek,Kim, Dae-Keun,Kim, Han-Sol,Kim, Won-Yong 한국재료학회 2011 한국재료학회지 Vol.21 No.5

The present study was carried out to evaluate the microstructural and mechanical properties of cross-roll rolled pure copper sheets, and the results were compared with those obtained for conventionally rolled sheets. For this work, pure copper (99.99 mass%) sheets with thickness of 5 mm were prepared as the starting material. The sheets were cold rolled to 90% thickness reduction and subsequently annealed at $400^{\circ}C$ for 30 min. Also, to analyze the grain boundary character distributions (GBCDs) on the materials, the electron back-scattered diffraction (EBSD) technique was introduced. The resulting cold-rolled and annealed sheets had considerably finer grains than the initial sheets with an average size of 100 ${\mu}M$. In particular, the average grain size became smaller by cross-roll rolling (6.5 ${\mu}M$) than by conventional rolling (9.8 ${\mu}M$). These grain refinements directly led to enhanced mechanical properties such as Vickers micro-hardness and tensile strength, and thus the values showed greater increases upon cross-roll rolling process than after conventional rolling. Furthermore, the texture development of <112>//ND in the cross-roll rolling processed material provided greater enhancement of mechanical properties relative to the case of the conventional rolling processed material. In the present study, we systematically discuss the enhancement of mechanical properties in terms of grain refinement and texture distribution developed by the different rolling processes.

마찰교반접합된 니켈기 초합금의 기계적 특성

송국현,Song, Kuk-Hyun,Nakata, Kazuhiro 한국재료학회 2011 한국재료학회지 Vol.21 No.7

This study was carried out to evaluate the microstructures and mechanical properties of a friction stir welded Ni based alloy. Inconel 600 (single phase type) alloy was selected as an experimental material. For this material, friction stir welding (FSW) was performed at a constant tool rotation speed of 400 rpm and a welding speed of 150~200 mm/min by a FSW machine, and argon shielding gas was utilized to prevent surface oxidation of the weld material. At all conditions, sound friction stir welds without any weld defects were obtained. The electron back-scattered diffraction (EBSD) method was used to analyze the grain boundary character distributions (GBCDs) of the welds. As a result, dynamic recrystallization was observed at all conditions. In addition, grain refinement was achieved in the stir zone, gradually accelerating from 19 ${\mu}m$ in average grain size of the base material to 5.5 ${\mu}m$ (150 mm/min) and 4.1 ${\mu}m$ (200 mm/min) in the stir zone with increasing welding speed. Grain refinement also led to enhancement of the mechanical properties: the 200 mm/min friction stir welded zone showed 25% higher microhardness and 15% higher tensile strength relative to the base material.

육성용접된 Inconel 718 합금의 마찰교반을 이용한 개질처리 효과

송국현,홍도형,양병모,Song, Kuk Hyun,Hong, Do Hyeong,Yang, Byung Mo 한국재료학회 2013 한국재료학회지 Vol.23 No.9

To evaluate the development of the microstructure and mechanical properties on surface modified and post-heattreated Inconel 718 alloy, this study was carried out. A friction stir process as a surface modification method was employed, and overlap welded Inconel 718 alloy as an experimental material was selected. The friction stir process was carried out at a tool rotation speed of 200 rpm and tool down force of 19.6-39.2 kN; post-heat-treatment with two steps was carried out at $720^{\circ}C$ for 8 h and $620^{\circ}C$ for 6 h in vacuum. To prevent the surface oxidation of the specimen, the method of using argon gas as shielding was utilized during the friction stir process. As a result, applying the friction stir process was effective to develop the grain refinement accompanied by dynamic recrystallization, which resulted in enhanced mechanical properties as compared to the overlap welded material. Furthermore, the post-heat-treatment after the friction stir process accelerated the formation of precipitates, such as gamma prime (${\gamma}^{\prime}$) and MC carbides, which led to the significant improvement of mechanical properties. Consequently, the microhardness, yield, and tensile strengths of the post-heat-treated material were increased more than 110%, 124% and 85 %, respectively, relative to the overlap welded material. This study systematically examined the relationship between precipitates and mechanical properties.

겹치기 마찰교반접합된 Inconel 600/SS 400 합금의 미세조직과 기계적 특성 평가

송국현,Song, Kuk-Hyun,Nakata, Kazuhiro 한국재료학회 2012 한국재료학회지 Vol.22 No.3

The microstructures and mechanical properties of friction stir welded lap joints of Inconel 600 and SS 400 were evaluated; friction stir welding was carried out at a tool rotation speed of 200 rpm and welding speed of 100 mm/min. Electron back-scattering diffraction and transmission electron microscopy were introduced to analyze the grain boundary characteristics and the precipitates, respectively. Application of friction stir welding was notably effective at reducing the grain size of the stir zone. As a result, the reduced average grain size of Inconel 600 ranged from $20{\mu}m$ in the base material to $8.5{\mu}m$ in the stir zone. The joint interface between Inconel 600 and SS 400 showed a sound weld without voids and cracks, and MC carbides with a size of around 50 nm were partially formed at the Inconel 600 area of lap joint interface. However, the intermetallic compounds that lead to mechanical property degradation of the welds were not formed at the joint interface. Also, a hook, along the Inconel 600 alloy from SS 400, was formed at the advancing side, which directly brought about an increase in the peel strength. In this study, we systematically discussed the evolution of microstructures and mechanical properties of the friction stir lap joint between Inconel 600 and SS 400.

교차롤압연된 Ni-Cr 합금의 기계적 특성 발달

송국현,김대근,손현택,이해진,김한솔,김원용,Song, Kuk-Hyun,Kim, Dae-Keun,Son, Hyun-Taek,Lee, Hae-Jin,Kim, Han-Sol,Kim, Won-Yong 한국재료학회 2011 한국재료학회지 Vol.21 No.10

We carried out this study to evaluate the grain refining in and the mechanical properties of alloys that undergo severe plastic deformation (SPD). Conventional rolling (CR) and cross-roll rolling (CRR) as SPD methods were used with Ni-20Cr alloy as the experimental material. The materials were cold rolled to a thickness reduction of 90% and subsequently annealed at $700^{\circ}C$ for 30 min to obtain a fully recrystallized microstructure. For the annealed materials after the cold rolling, electron back-scattered diffraction (EBSD) analysis was carried out to investigate the grain boundary characteristic distributions (GBCDs). The CRR process was more effective when used to develop the grain refinement relative to the CR process; as a result, the grain size was refined from $70{\mu}m$ in the initial material to $4.2{\mu}m$ (CR) and $2.4{\mu}m$ (CRR). These grain refinements have a direct effect on improving the mechanical properties; in this case, the microhardness, yield and tensile strength showed significant increases compared to the initial material. In particular, the CRR-processed material showed more effective values relative to the CR-processed materials. The different texture distributions in the CR (001//ND) and CRR (111//ND) were likely the cause of the increase in the mechanical properties. These findings suggest that CRR can result in materials with a smaller grain size, improved texture development and improved mechanical properties after recrystallization by a subsequent annealing process.

교차롤압연된 Ni-10Cr 합금의 결정립 미세화와 성형성 향상

송국현,김원용,손현택,Song, Kuk-Hyun,Kim, Won-Yong,Son, Hyun-Taek 한국재료학회 2012 한국재료학회지 Vol.22 No.6

This study evaluated the enhancement of microstructural and mechanical properties of a cross rolled Ni-10Cr alloy, comparing with conventionally rolled material. Cold rolling was carried out to 90% thickness reduction and the specimens were subsequently annealed at $700^{\circ}C$ for 30 min to obtain a fully recrystallized microstructure. Cross roll rolling was carried out at a tilted roll mill condition of $5^{\circ}$ from the transverse direction in the RD-TD plane. In order to observe the deformed microstructures of the cold rolled materials, transmission electron microscopy was employed. For annealed materials after rolling, in order to investigate the grain boundary characteristic distributions, an electron back-scattering diffraction technique was applied. Application of cold rolling to the Ni-10Cr alloy contributed to notable grain refinement, and consequently the average grain size was refined from 135 ${\mu}m$ in the initial material to 9.4 and 4.2 ${\mu}m$ in conventionally rolled and cross rolled materials, respectively, thus showing more significantly refined grains in the cross rolled material. This refined grain size led to enhanced mechanical properties such as yield and tensile strengths, with slightly higher values in the cross rolled material. Furthermore, the <111>//ND texture in the CRR material was better developed compared to that of the CR material, which contributed to enhanced mechanical properties and formability.

강소성 가공된 Ni-30Cr 합금의 결정립 미세화와 기계적 물성 향상

송국현 ( Kuk Hyun Song ),김한솔 ( Han Sol Kim ),김원용 ( Won Yong Kim ) 대한금속재료학회(구 대한금속학회) 2011 대한금속·재료학회지 Vol.49 No.8

The present study evaluated the microstructures and mechanical properties of severely deformed Ni-30Cr alloys. Cross-roll rolling (CRR) process was introduced as a severe plastic deformation (SPD), and Ni-30Cr alloy sheets were cold rolled to 90% thickness reduction and subsequently annealed at 700℃ for 30 min to obtain the recrystallized microstructure. Electron back-scattering diffraction (EBSD) was introduced to analyze grain boundary character distributions (GBCDs). The application of CRR to the Ni-30Cr alloy was effective in enhancing the grain refinement through heat treatment; consequently, the average grain size was significantly refined from 33㎛in the initial material to 0.6㎛. This grain refinement directly improved the mechanical properties, in which yield and tensile strengths significantly increased relative to those of the initial material. We systematically discuss the grain refinement and accompanying improvement of the mechanical properties, in terms of the effective strain imposed by CRR relative to conventional rolling (CR).

마찰접합 된 STK400 Tube의 미세조직과 기계적 특성 평가

김경우,송국현,Kim, Gyeong-Woo,Song, Kuk-Hyun 한국재료학회 2019 한국재료학회지 Vol.29 No.1

We evaluate the properties of friction welded STK400 steel tube in terms of the relationship between microstructures and mechanical properties. Friction welding is conducted at a rotation speed of 1,600 rpm and upset time of 3-7 sec for different thicknesses of STK 400 tubes. To analyse the grain boundary characteristic distributions(GBCDs) in the welded zone, electron backscattering diffraction(EBSD) method is introduced. The results show that a decrease in welding time (3 sec.) creates a notable increase grain refinement so that the average grain size decreases from $15.1{\mu}m$ in the base material to $4.5{\mu}m$ in the welded zone. These refined grains achieve significantly enhanced microhardness and a slightly higher yield and higher tensile strengths than those of the base material. In particular, all the tensile tested specimens experience a fracture aspect at the base material zone but not at the welded zone, which means a soundly welded state for all conditions.

이주속압연된 Ni-30Cr 합금의 미세조직과 기계적 특성 발달

임용덕,박형기,송국현,Im, Yong-Deok,Park, Hyung-Ki,Song, Kuk-Hyun 한국재료학회 2015 한국재료학회지 Vol.25 No.3

We evaluated the developed microstructures and mechanical properties of a severely plastically deformed Ni-30Cr alloy. Normal rolling and differential speed rolling were used as deformation processes, and the thicknesses of the specimens were reduced to 68 % of the original thickness after holding at $700^{\circ}C$ for 10 min and annealing at $700^{\circ}C$ for 40 min to obtain a fully recrystallized microstructure. Electron backscattering diffraction was used to analyze the characteristic distribution of the grain boundaries on the deformed and annealed specimens. Differential speed rolling was more effective for refining grains in comparison with normal rolling. The grain size was refined from 33 mm in the initial material to 8.1 mm with normal rolling and 5.5 mm with differential speed rolling. The more refined grain in the differential-speed-rolled material directly resulted in increases in the yield and tensile strengths by 68 % and 9.0%, respectively, compared to normal rolling. We systematically explain the relationship between the grain refinement and mechanical properties through a plastically deformed Ni-30Cr alloy based on the development of a deformation texture. The results of our study show that the DSR process is very effective when used to enhance the mechanical properties of a material through grain refinement.

체간부 유건종(Desmoid Tumor) 7예

구자현(Ja Hyun Koo),강구정(Koo Jeong Kang),송국현(Kuk Hyun Song),박성대(Sung Dae Park),정기용(Ki Yong Chung) 대한외과학회 1999 Annals of Surgical Treatment and Research Vol.56 No.1