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청국장 향미에 미치는 ${\beta}-cyclodextrin$의 포접 효과
이인선,김순미,김혜영B,Lee, In-Seon,Kim, Soon-Mi,L. Kim, Hye-Young 한국식생활문화학회 2001 韓國食生活文化學會誌 Vol.16 No.4
식품의 향기를 포접하여 향기성분을 순화시키는 성질을 지닌 ${\beta}-cyclodextrin$을 청국장에 0%, 10%, 20% 및 30%씩 첨가하여 청국장의 냄새에 대한 포접효과를 살펴보면, ${\beta}-cyclodextrin$을 20% 대체한 시료의 단백질과 회분양은 control 시료보다 유의적으로 감소하였다. 지방량과 탄수화물량은 대체시료가 control 시료보다 유의적으로 증가하였다. 시료의 L값은 ${\beta}-cydodextrin$을 30%대체한 시료가 53.99로 가장 밝게 평가되었고, 대체수준이 10%일 때 L값은 51.81으로 유의적으로 가장 낮은 수치를 보이며 색이 더 진하게 평가 되었다. 시료의 a값은 대체 수준이 증가할수록 감소하여 붉은 정도가 옅어지었다. 시료의 b값은 대체량이 증가할수록 시료의 노란정도가 점점 옅어짐을 나타내었다. 시료 입자의 내부구조 조직을 주사전자 현미경으로 관찰한 결과, control 시료의 내부구조는 점질물질이 불규칙 한 모양으로 뭉쳐져 있거나 거칠게 퍼져 있음을 볼 수 있었으며, 첨가수준이 증가할수록 불규칙하고 거친 내부조직이 점차 감소하여 30% 대체 시료에서는 매끈하고 안정된 조직감과 내부구조를 보여 주었다. 관능적 특성에 대한 결과, 청국장 시료의 구수한 냄새는 시료의 대체수준이 20% 이상으로 될 때 구수한 냄새는 6.65에서 6.78의 수치를 보이며 유의적으로 다소 감소하여 구수한 냄새가 약하게 나타났다. 시료의 이취는 ${\beta}-cyclodextrin$을 대체량을 20%로 증가한 시료에서 control 시료의 이취보다 유의적인 감소를 보여 주었다. (p<0.05). 시료의 짠맛은 20% 대체시료군이 control 시료의 짠맛보다 유의적으로 현저히 감소하였으며, 쓴맛은 control 시료에 비하여 모든 대체시료군이 낮은 수치로 쓴맛이 약해지는 경향을 나타내었다. 이상으로 ${\beta}-cyclodextrin$으로 청국장을 포접시엔 특히, 구수한 냄새 이취 및 짠맛을 순화하는 경향이 있는 것을 알 수 있었다. Flavor modifing effects of ${\beta}-cyclodextrin$ on the flavor of Chungkookjang(Korean traditional fermented bean paste) were investigated with varied substitution levels of 10, 20, and 30%. The 20% substituted sample groups showed significantly lower amount of protein and ash contents compared to those of control. The L value of brightness had significantly the largest value of 53.99 with 30% substituted sample group, and lower a and b values. Internal structures of control group observed using the scanning electronic microscope, had irregular round type shape with viscous materials, and they had tendencies to be less rough and organized making even and ordered internal cell structures as the substituted levels were increased. Results of sensory characteristics showed significantly lower off-odor and salty flavor with the 20% substituted sample groups compared to those of control. Results of this study showed the possibilities of flavor moderating effects of ${\beta}-cyclodextrin$ when it was used as one of the flavor modifier of the Chungkookjang. Future studies of finding the optimum level of substitution is further required.
연구논문 : 국내산 및 수입산 천일염 이용 배추김치의 저장 중 품질특성
김혜영 ( In Seon Lee ),이인선 ( Hyang Sook Kim ),김향숙 ( Hae Young Kim ) 한국식품조리과학회(구 한국조리과학회) 2012 한국식품조리과학회지 Vol.28 No.4
Quality characteristics of baechu (Kimchi cabbage) kimchi prepared using various kinds of domestic solar salts (KS5Y, KS2Y, KS1Y, KFS, and KSS) and imported solar salts (AS1Y and CS1Y) were compared with Korean processed salt (KRS) and Mexican rock salt (MR1Y) during 60 days of storage. Sodium contents of MR1Y, AS1Y, and domestic KRS with values of 363,653.40, 358,952.40, and 356,799.90 mg/dL, respectively, were significantly higher than that of KFS with a value of 280,249.80 mg/dL (p < 0.001). Thus, the kimchi using KFS was expected to have 22-23% lower sodium content compared to that of the other kimchis. KFS magnesium content was significantly highest at 4,464.10 mg/dL and calcium was significantly the highest in samples of KS1Y with a value of 711.31 mg/dL. Most of the pHs and acidities in the kimchi samples were in the optimum range due to the relatively low storage temperature of 2℃. The salt concentrations of all kimchis using domestic solar salt during storage was greatly reduced compared to those using the imported salts or KRS. Sensory saltiness of the KS1Y sample group was significantly the lowest value (6.08) at 0 days of storage (p < 0.001) and maintained relatively low saltiness during the entire storage period. The crispness of the KS2Y, KS1Y, and KSS sample groups were significantly higher (10.02, 9.77, and 9.49, respectively), compared to that of KRS (7.64) at 60 days of storage (p < 0.001). The KFS sample group had the higher acceptance values for pickled seafood aroma, sour aroma, saltiness, and overall acceptability compared to those in the other samples.
연구논문 : 매운맛 등급화 고춧가루로 제조한 배추김치의 이화학적 관능적 특성
이인선 ( In Seon Lee ),이연경 ( Yeon Kyeong Lee ),김혜영 ( Hae Young Kim ) 한국식품조리과학회(구 한국조리과학회) 2014 한국식품조리과학회지 Vol.30 No.1
This study investigated the spicy hot flavor related quality characteristics of baechu (Kimchi cabbage) Kimchi prepared using hot pepper powder in various capsaicin levels during 8 weeks of storage. The pHs in the Kimchi samples were in the optimum range of the pH 4.2-4.5 due to the relatively low storage temperature of 2℃ during the entire storage periods. The L, a and b values of cap-150 sample group were significantly higher compared to those in the other samples at 8 weeks of storage. Grading hotness of the Kimchi was significantly clearly separated when varied levels of hotness for the hot pepper powder were used at 2-4 weeks of storage (p<0.001). Sensory spicy hotness of the cap-40 showed significantly the lowest with values of 4.57-4.38 representing mild hot; that of cap-85 was medium hot with values of 5.81-6.00; and finally, that of cap-150 showed the values of 6.86-7.14, representing strong hot flavor at 2-4 weeks of storage (p<0.001). The grading of spicy hotness in the Kimchi increased by about one level at the optimal edible periods due to the leaching out of capsaicin from the hot pepper powder for those storage periods. Thus, the increased hotness of the Kimchi in the optimal edible periods should be considered when the desired hotness of the hot pepper is chosen for the Kimchi preparation. The hotness decreased as the organic acids were generated during ripening by the 8th week of storage.
ε-Caprolactam과 2-Piperidone으로부터 나일론 6,5 공중합체 제조 및 특성평가
김혜영(Hye Young Kim),고진선(Jin Seon Goh),류미회(Mi Hee Ryu),김대수(Dae Su Kim),송봉근(Bong Keun Song),이승환(Seung Hwan Lee),박시재(Si Jae Park),제갈종건(Jong Geon Jegal) 한국고분자학회 2014 폴리머 Vol.38 No.1
본 연구에서는 바이오매스 기반 나일론 6,5 공중합체를 제조하기 위하여 단량체인 ε-caprolactam과 2-piperidone을 glucose로부터 발효공정으로 제조된 lysine과 5-aminovaleric acid로부터 각각 제조하였다. 이들을 potassium tertbutoxide를촉매로 하고 acetyl-2-caprolactam과 이산화탄소를 개시제로 사용하여 40 oC에서 음이온 개환 중합 방법을 이용하여 나일론 6,5 공중합체를 제조하였다. 제조된 바이오 나일론 6,5 공중합체의 특성을 여러 가지 기기분석방법으로 분석하였다. 이때 얻어진 고분자의 점도분자량(Mη)은 최대 30000 g/mol 정도였으며, 중합 수율은 50% 이상이었다. 이들은 모두 semi-crystalline 고분자로 밝혀졌다. 열 특성 분석 결과 용융온도는 약 165 oC 정도로 분해온도 250 oC와 큰 차이를 나타내었다. 이들 고분자들은 우수한 가공성과 응용성을 지닐 것으로 예상된다. To prepare biomass based nylon 6,5 copolymers, ε-caprolactam and 2-piperidone, the monomers of nylon 6,5copolymers, were synthesized respectively from lysine and 5-aminovaleric acid which were produced from glucose bythe fermentation process. The copolymers were then polymerized by the anionic ring opening polymerization of them at40 oC, using potassium tert-butoxide as a catalyst and acetyl-2-caprolactam and carbon dioxide as initiators. The preparedcopolymers were characterized with various analytical methods: their viscosity molecular weight (Mη) was as high as30000 g/mol and polymerization yield was over 50%, and it was found that they were semi-crystalline polymers havingmelting point at 165 oC which was much lower than its thermal degradation point, 250 oC. These polymers were expectedto have good thermal processability and application fields.
인천연안 Vibrio parahaemolyticus의 분포 및 유산과 과산화수소 처리에 의한 항균효과
장재선,조우균,이혜정,이제만,김혜영,김용희,Jang, Jae-Seon,Cho, Woo-Kyoun,Lee, Hye-Jeong,Lee, Jea-Mann,Kim, Hye-Young,Kim, Yong-Hee 대한환경위생공학회 2006 대한환경위생공학회지 Vol.21 No.4
This study was carried out to investigate the distribution of Vibrio parahaemolyticus in the Incheon adjacent sea, and antimicrobial effect on growth of Vibrio parahaemolyticus in lactic acid and hydrogen peroxide and combination of lactic acid and hydrogen peroxide. The detected strains were compared geographical, months and sample types. The distribution of Vibrio parahaemolyticus was high at Ganghwa county with 66.1%(336 samples), on 7-9 months with 72.4%(386 samples) and from tireland with 75.0%(90 samples), respectively. The minimun inhibitory concentration (MIC) of lactic acid in Vibrio parahaemolyticus were 1250 ppm at pH 6.5 and 7.0, 625 ppm at pH 6.0. respectively. The minimun inhibitory concentration (MIC) of hydrogen peroxide in Vibrio parahaemolyticus were 25 ppm at pH 6.5 and 7.0, 12.5 ppm at pH 6.0, respectively. MICs of combined treatment of lactic acid and hydrogen peroxide in Vibrio parahaemolyticus were 625 ppm of lactic acid with 12.5 ppm of hydrogen peroxide. The correlations between MICs of lactic acid and hydrogen peroxide in Vibrio parahaemolyticus were obtained through the coefficient of determination($R^2$). $R^2$ value were 1.0000. The antimicrobial effect of lactic acid and hydrogen peroxide in Vibrio parahaemolyticus could be confirmed from the result of this experiment.