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Microstructural evolution and fracture toughness of Al₂O₃/Ti composites
M. Vázquez-Villar,M. Romero-Romo,A. Altamirano-Torres,E. Rocha-Rangel 한양대학교 세라믹연구소 2008 Journal of Ceramic Processing Research Vol.9 No.3
The effect of different additions of a metal (Ti) on the microstructure and fracture toughness of Al2O3-based ceramics, as well as the establishment of a route for their processing was analyzed in this study. The samples were prepared by means of mechanical milling and pressureless sintering in an argon atmosphere. Due to the fact of working with very small sizes of powders of both the metal and ceramic, it was possible to reach in sintered products greater values of densification than 95% of their relative density. Measurements of fracture toughness (KIC) evaluated by the fracture indentation method, indicate that this mechanical property had improved with some additions of Ti in the composite, for example KIC for pure alumina processed under the conditions of this study was 3.0MPa·m1/2, whereas, KIC for the composite with 3 vol % Ti was 4.1MPa·m1/2. The microstructure observed in a scanning electron microscopy shows the formation of small and fine metallic interpenetrating networks in the ceramic matrix, that improve in their formation with an increases of Ti in the composite. The effect of different additions of a metal (Ti) on the microstructure and fracture toughness of Al2O3-based ceramics, as well as the establishment of a route for their processing was analyzed in this study. The samples were prepared by means of mechanical milling and pressureless sintering in an argon atmosphere. Due to the fact of working with very small sizes of powders of both the metal and ceramic, it was possible to reach in sintered products greater values of densification than 95% of their relative density. Measurements of fracture toughness (KIC) evaluated by the fracture indentation method, indicate that this mechanical property had improved with some additions of Ti in the composite, for example KIC for pure alumina processed under the conditions of this study was 3.0MPa·m1/2, whereas, KIC for the composite with 3 vol % Ti was 4.1MPa·m1/2. The microstructure observed in a scanning electron microscopy shows the formation of small and fine metallic interpenetrating networks in the ceramic matrix, that improve in their formation with an increases of Ti in the composite.
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Dasgupta-Schubert, N.,Tiwari, D.K.,Francis, E. Reyes,Martinez Torres, P.,Villasenor Cendejas, L.M.,Lara Romero, J.,Villasenor Mora, C. Techno-Press 2017 Advances in nano research Vol.5 No.3
Multiwalled carbon-nanotubes (MWCNT) and micro-structured carbon, such as biochar or activated carbon (AC), have been seen to significantly increase the growth indices of certain plant species such as maize (Zea mays L.). Seed imbibition is the stage where environmental factors that affect water transport across the seed coat barrier, make a large impact. This work explores the effect on water imbibition by maize seeds when the aqueous environment surrounding the seed is diluted by small concentrations (10 and 20 mg/l) of pristine MWCNT (p-MWCNT), carboxylate functionalized MWCNT (COO-MWCNT) and AC. The degree of sensitivity of the process to (i) large structural changes is seen by utilizing the nano (the MWCNT) and the micro (the AC) allotropic forms of carbon; (ii) to small changes in the purity and morphology of the p-MWCNT by utilizing 95% pure and 99% pure p-MWCNTs of slightly differing morphologies; and (iii) to MWCNT functionalization by using highly pure (97%) COO-MWCNT. Water imbibition was monitored over a 15 hour period by Near Infrared Thermography (NIRT) and also by seed weighing. Seed surface topography was seen by SEM imaging. Analysis of the NIRT images suggests rapid seed surface topological changes with the quantity of water imbibed. While further work is necessary to arrive at a conclusive answer, this work shows that the imbibition phase of the maize seed is sensitive to the presence of MWCNT even to small differences in the purity of the p-MWCNT and to small differences in the physicochemical properties of the medium caused by the hydrophilic COO-MWCNT.
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Ramiro Guerrero-Santos,Gabriela Cabrales-Orona,John Paul Délano-Frier,Judith Cabello-Romero,José Román Torres-Lubián,José Humberto Valenzuela-Soto 한국식물병리학회 2024 Plant Pathology Journal Vol.40 No.1
Huanglongbing (HLB) is a disease caused by the phloem- limited Candidatus Liberibacter asiaticus (CLas) that affects the citrus industry worldwide. To date, only indirect strategies have been implemented to eradicate HLB. Included among these is the population control of the psyllid vector (Diaphorina citri), which usually provides inconsistent results. Even though strategies for direct CLas suppression seem a priori more promising, only a handful of reports have been focused on a confrontation of the pathogen. Recent developments in polymer chemistry have allowed the design of polycationic self-assembled block copolymers with outstanding antibacterial capabilities. Here, we report the use of polymeric nano-sized bactericide particles (PNB) to control CLas directly in the phloem vasculature. The field experiments were performed in Rioverde, San Luis Potosí, and is one of the most important citrusproducing regions in Mexico. An average 52% reduction in the bacterial population was produced when PNB was injected directly into the trunk of 20 infected trees, although, in some cases, reduction levels reached 97%. These results position PNB as a novel and promising nanotechnological tool for citrus crop protection against CLas and other related pathogens.
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Tahali Mendoza-Oliveros,Victor Arana-Argáez,Leidi C. Alvaréz-Sánchez,Julio Lara-Riegos,María Elizbeth Alvaréz-Sánchez,Julio C. Torres-Romero 대한기생충학ㆍ열대의학회 2019 The Korean Journal of Parasitology Vol.57 No.1
Trichomoniasis is a common sexually transmitted infection caused by Trichomonas vaginalis, which actually does not exist a vaccine for control or prevention. Thus, the identification of new and potent immunogens in T. vaginalis, which can contribute to the development of a vaccine against this parasite, is necessary. Therefore, the aim of this work was to evaluate the potential of a recombinant Transient Receptor Potential-like channel of T. vaginalis (TvTRPV), as a promising immunogen in BALB/c mice. First, TvTRPV was cloned and expressed as a recombinant protein in Escherichia coli BL21 cells and purified by nickel affinity. Next, BALB/c mice were immunized and the antibody levels in mice serum and cytokines from the supernatant of macrophages and from co-culture systems were evaluated. Recombinant TvTRPV triggered high levels of specific total IgG in sera from the immunized mice. Also, a statistically significant increase of cyto- kines: IL-1β, IL-6, and TNF-α after stimulation with the corresponding antigens in vitro, was identified. Moreover, co-cul- tures using CD4+ T cells from immunized mice were able to identify higher levels of IL-10 and IFN-γ. These results were useful to validate the immunogenicity of TvTRPV in BALB/c mice, where IL-10-IFN-γ-secreting cells could play a role in infection control, supporting the potential of TvTRPV as a promising target for vaccine against T. vaginalis.
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