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- 저자 : Castillo-Ojeda (검색결과 2 건)
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Structural and optical characterization of wurtzite type ZnS
J. Díaz-Reyes,R.S. Castillo-Ojeda,R. Sánchez-Espíndola,M. Galván-Arellano,O. Zaca-Morán 한국물리학회 2015 Current Applied Physics Vol.15 No.2
ZnS films were grown on (001) GaAs substrates at different temperatures by RF magnetron sputtering. The ZnS chemical stoichiometry was determined by Energy-dispersive X-ray spectroscopy (EDS), besides it allowed to find the residual impurities, mainly oxygen. The X-ray diffraction (XRD) analysis and Raman scattering reveal that ZnS deposited thin films showed hexagonal wurtzite crystalline phase. The films average crystallite size range was from 8.15 to 31.95 nm, which was determined using the Debye eScherrer equation for the peak W(101). Besides an experimental study of first- and second-order Raman scattering of ZnS films is made. An energy level diagram involving oxygen traps and interstitial sulphur ions is used to explain the origin of the radiative transitions observed in the room temperature photoluminescence (PL) spectra.
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Characterization of CBD-CdSe1-ySy deposited at low-temperature for photovoltaic applications
J.I. Contreras-Rascón,J. Díaz-Reyes,J.E. Flores-Mena,M. Galvan-Arellano,L.A. Juárez-Morán,R.S. Castillo-Ojeda 한국물리학회 2015 Current Applied Physics Vol.15 No.12
We present the structural and optical characterization of cadmium selenide sulphur (CdSe1-ySy) deposited by chemical bath deposition (CBD) technique at low-temperature (20 ± 2 ℃). The sulphur molar fraction is varied from 0 to 42.13%. The chemical stoichiometry is estimated by energy-dispersive X-ray spectroscopy (EDS). The CdSe1-ySy shows hexagonal wurtzite crystalline phase, which was found by X-ray diffraction (XRD) analysis and it was confirmed by Raman spectroscopy. The average grain size of the CdSe1-ySy films was ranged from 1.20 to 1.68 nm that was determined by Debye-Scherrer equation from W(002) direction and it was confirmed by high resolution transmission electron microscopy (HRTEM). This average grain size indicates a high quantum confinement because of it is smaller than the Bohr radii of CdS (2.8 nm) and CdSe (4.9 nm). Raman spectra show two dominant vibrational bands about 208 and 415 cm-1 associated at CdSe-1LO-like and CdSe-2LO-like. By transmittance measurements at room temperature are found that the optical band gap energies vary from 1.86 to 2.16 eV in the range of investigated sulphur molar fraction. Room temperature photoluminescence shows radiative bands in the visible range and a dominant band in the UV range, approximately 3.0 eV, which can be associated with a radiative transition, bound exciton to donor impurity.
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