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Homologous 산화물 Zn<sub>k</sub>In<sub>2</sub>O<sub>3+k</sub>(k=1∼9)의 열전 특성
남윤선,최정규,홍정오,이영호,이명현,서원선,Nam, Yun-Sun,Choi, Joung-Kyu,Hong, Jeong-Oh,Lee, Young-Ho,Lee, Myung-Hyun,Seo, Won-Seon 한국재료학회 2003 한국재료학회지 Vol.13 No.8
In order to investigate the thermoelectric properties of $Zn_{k}$ $In_2$$O_{ 3+k}$ homologous compounds, the samples of $Zn_{k}$ /$In_2$$O_{3+k}$ / (k = integer between 1 and 9) were prepared by calcining the mixed powders of ZnO and $In_2$$O_3$fellowed by sintering at 1823 K for 2 hours in air, and their electrical conductivities and Seebeck coefficients were measured as a function of temperature in the range of 500 K to 1150 K. X-ray diffraction analysis of the sintered samples clarified that single-phase specimens were obtained for $Zn_{k} /$In_2$$O_{3+k}$ with k = 3, 4, 5, 7, 8, 9. Electrical conductivity of the $Zn_{k}$ $In_2$$O_{3+k}$ / decreased with increasing temperature, and decreased with increasing k for k $\geq$ 3. The Seebeck coefficient was negative at all the temperatures for all compositions, confirming that $Zn_{k}$ $In_2$$O_{3+k}$ / is an n-type semiconductor. Absolute values of the Seebeck coefficient increased linearly with increasing temperature and increased with increasing k for k $\geq$ 3. The temperature dependence of the Seebeck coefficient indicated that Z $n_{k}$I $n_2$ $O_{3+k}$ could be treated as an extrinsic degenerate semiconductor. Figure-of-merits of Z $n_{k}$I $n_2$ $O_{3+k}$ were evaluated from the measured electrical conductivity and Seebeck coefficient, and the reported thermal conductivity. Z $n_{7}$ I $n_2$ $O_{10}$ has the largest figure-of-merit over all the temperatures, and its highest value was $1.5{\times}$10$^{-4}$ $K^{-1}$ at 1145 K.5 K.
고상법에 의한 100 nm BaTiO<sub>3</sub> 분말의 합성
김정환,정한승,조준엽,홍정오,김영태,허강헌,Kim, Jung-Hwan,Jung, Han-Seong,Cho, Joon-Yeob,Hong, Jeong-Oh,Kim, Young-Tae,Hur, Kang-Heon 한국세라믹학회 2009 한국세라믹학회지 Vol.46 No.2
$BaTiO_3$ powder was synthesized by the solid-state reaction of fine $BaTiO_3$ and $TiO_2$ raw materials. Fine grinding media of 50 and 300 microns were used for obtaining fine particulate mixture of $BaTiO_3$ and $TiO_2$ with high homogeneity. Effect of the size of grinding media on the synthesis mechanism of $BaTiO_3$ was discussed on the basis of the particulate morphology and thermogravimetry data for the mixture powders. By using the finer grinding media, $BaTiO_3$ was formed at the lower temperature and the particle size with the relatively narrower distribution could be obtained. $BaTiO_3$ powder with the average size of 100 nm was synthesized by the solid reaction in vacuum atmosphere.