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파인 세라믹의 분석을 위한 알칼리 용융법과 고압 산분해법의 비교 및 응용
임흥빈,한정란,이계호,이광우,유택아명,Im, Heung Bin,Han, Jeong Ran,Lee, Gye Ho,Lee, Gwang U,Yu, Taek A Myeong 대한화학회 1994 대한화학회지 Vol.38 No.6
난용성 신소재 중의 하나인 파인 세라믹의 분석을 위하여, 알칼리 용융법과 고압 산분해법 등의 시료 전처리법을 유도결합원자발광분석기(ICP-AES)를 이용하여 연구하였다. Al2O3 분말을 분석하여 본 결과, 고압 산분해법이 알칼리 용융법보다 재현성 있는 측정치를 얻을 수 있었다. SiC분말의 경우에서는 고압산분해법으로 처리한 후 Si매트릭스를 Si-F형태로 증발시켜서 분석하여 본 결과 분말 중의 ppm 농도 범위의 불순물들이 매트릭스에 의한 간섭없이 분석되었다. 일본 인증기준물인 JCRM022, JCRM023 초미립 분말을 고압 산분해법으로 분석하여 본 결과, 좋은 재현성과 높은 정확성을 나타내었다. For the analysis of fine ceramics, which is one of the new materials difficult to be dissolved, the methods of sample pretreatments such as alkali fusion and high pressure acid digestion were studied using inductively coupled plasma-atomic emission spectrometer(ICP-AES). For the Al2O3 powder sample, the results from high pressure acid digestion method showed better reproducibility than those obtained by alkali fusion technique. In the case of the analysis of SiC powder using the former method, impurities of the powder in the range of ppm were determined without matrix interference by removing Si as Si-F volatilization. Japan Certified Reference Materials (JCRM022 and JCRM023) were analyzed by this method for ultra fine powder and the results showed high accuracy and good reproducibility.
$La(OH)_3$ 공침에 의한 해수중 흔적량 코발트, 구리, 및 전체 크롬의 동시 부선 및 정량
조만식,임흥빈,김영상,Jo, Man Sik,Im, Heung Bin,Kim, Yeong Sang 대한화학회 1994 대한화학회지 Vol.38 No.9
The precipitate flotation using $La(OH)_3$ as a coprecipitant was studied for the simultaneous determination of trace three elements in a sea water. Several experimental conditions such as pH, coprecipitant and surfactant were investigated with an artificial sea water. To remove the influence of Cr(VI) the Cr(VI) was reduced to Cr(III) using $NaBH_4$ prior to the flotation. Trace amounts of Cu(II), Co(II) and total Cr in 1.0 l sea water was coprecipitated together with the precipitation of $La(OH)_3$ in the solution of pH 9.8 adjusted with 3.OM NaOH solution. The precipitate was floated by using a mixed surfactant (1 to 8 of each 0.5% ethanolic sodium oleate and sodium dodecylsulfate solution) by bubbling a nitrogen gas. The floats was separated and filtrated from the mother liquor by suction. The precipitate was dissolved in 7.0 M $HNO_3$ solution and then marked to 25.0 ml with a deionized water. These elements were determined by graphite fumace atomic absorption spectrophotometry. This method was applied to determine the elements in the sea water of the Eastern and Western coasts. And the recoveries were over 90.0% in the samples into which given amounts of the analyte elements were spiked. $La(OH)_3$를 공침제로 사용하여 해수중 흔적량 세 가지 원소를 동시에 부선시켜 정량하는 방법에 관하여 연구하였다. 인공해수를 사용하여 효과적인 부선을 위한 용액의 pH, 공침제의 양, 계면활성제의 종류와 양 등의 실험조건을 최적화시켰다. 부선하기 전에 Cr(VI)를 $NaBH_4$에 의하여 Cr(III)으로 환원시켜 크롬이 공침되도록 하였다. 해수시료 1.0 l에 $La^{3+}$를 가하고 용액의 pH를 9.8로 조절하여 $La(OH)_3$로 침전시키면서 흔적량 Co(III), Cu(II) 및 Cr(Ⅲ)이 공침되게 하였다. 부피 1:8의 0.5% sodium oleate와 sodium dodecylsulfate 에탄올 용액을 가하고 질소기체로 bubbling하여 침전들을 띄웠다. 뜬 침전을 분리해 내어 걸르고 씻은 다음 7.0 M $HNO_3$ 용액으로 녹여서 탈염수로 묽혀 25.0 ml가 되게 하였다. 분석원소들을 흑연료 원자흡수 분광광도법으로 정량하는데 인공해수로 표준용액을 만들어 검정곡선을 작성하였다. 이 방법을 동해와 서해의 물시료중 이들 원소분석에 응용하여 좋은 결과를 얻었다. 그리고 해수시료에 이들 원소를 일정량 첨가하여 얻은 회수율은 90.0% 이상으로 본 방법이 정량적임을 확인하였다.
최정인(Jeong-in Choi),임흥빈( Heung-bin Im),정은희(Eun-hee Jung),김태열(Tae-yuel Kim),손영금(Yeong-geum Son),고순미(Sun-mi Ko),이호정(Ho-jung Lee),오조교(Jo-gyo Oh) 한국환경보건학회 2018 한국환경보건학회지 Vol.44 No.4
Objectives: A lake is a place used by many people, and compared to rivers it is easy for them to become polluted. The water quality in lakes and reservoirs has been worsening recently. The purpose of this study is to evaluate the water pollution characteristics of major lakes in northern Gyeonggi-do Province. Methods: Six lakes were selected as major lakes and were evaluated in terms of water pollution characteristics and eutrophication (as defined by results for COD Mn , TOC, SS, Chl-a, T-N and T-P) over one year (from December 2016 through November 2017) in northern Gyeonggi-do Province. Results: The annual average COD Mn was found to be 3.1 mg/L in Onam, 3.6 mg/L in Sanjeong, 4.7 mg/L in Gisan, 4.8 mg/L in Ilsan, and 6.1 mg/L in Jangja. The results of the Korean trophic state index (TSI KO ) value indicated a eutrophic state (TSI KO 59.0) in Jangja lake. The other lakes were classified as being in a mesotrophic state (TSI KO of 38.1 in Sanjeong, 40.2 in Ilsan, 41.9 in Onam, 46.1 in Gisan, and 47.8 in Gomo). Conclusions: Ilsan Lake’s water quality is being well maintained. Sanjeong, Onam, and Gisan are appropriate for use as agricultural water. Jangja lake requires efforts for water quality improvement and to prevent the inflow of non-point pollutant sources.
손영금(Yeong-Geum Son),임흥빈(Heung-Bin Im),이강혁(Kang-Hyuck Lee),김진길(Jin-Guil Kim),임윤정(Yun-Jung Im),최정인(Jeong-In Choi),이호정(Ho-Jung Lee),오조교(Jo-Gyo Oh) 한국환경보건학회 2017 한국환경보건학회지 Vol.43 No.5
The objective of this study is to evaluate and analyze Sincheon basin water environment system. The data were collected from 2010 August to 2016 December including BOD, SS, T-N, T-P. The results were as followed. As the result of comparing the amount of BOD generated by pollution sources in the Sincheon water system, industrial was the highest at 33,259.4 kg/day. In comparison with the tributary, it was estimated that Dong-Du water system reveals the highest level of BOD in the industry. Population and livestock was high in CheongDam and Sang-Pae water system. With the inflow stream of Hyo-Chon, Suk-Woo and Sang-Pae, the pollution degree of BOD and T-N level of Sincheon increased and pollution degree of tributary was higher than that of Sincheon’s main stream. The main reason of pollutant of Suk-Woo was from untreated wastewater, and it influenced downstream of Suk-Woo. Hyo-Chon stream satisfy the water quality standard, but Zn was designated as a Monitoring contaminants, was high as 14.670 mg/L (standard 0.02~2.45mg/L)because of textile wastewater. And Sang-Pae stream was polluted by livestock wastewater of livestock farms as a nonpoint source.
QGIS를 이용한 경기도내 토양오염원의 중점관리 지점 선정
손영금(Yeong-Geum Son),김지영(Ji-Young Kim),박진호(Jin-Ho Park),임흥빈(Heung-Bin Im),김종수(Jong-Su Kim) 한국환경보건학회 2020 한국환경보건학회지 Vol.46 No.1
Object: The purpose of this study was to select priority points for soil management using the location of groundwater and to suggest this method for soil contamination surveys. Method: Groundwater impact range was set to an area of 100 to 500 meters from the center point of agricultural groundwater wells. Data on industrial complex and factory areas, areas of stored or used ores and scrap metals, areas associated with waste and recycling, and traffic-related facilities areas were collected and checked for whether they fall within the groundwater impact range. Longitude and latitude coordinates of these data were mapped on the groundwater impact range using QGIS (Quantum Geographic Information System). Results: Considering the groundwater impact range, the points were selected as follows: 589 points were selected from 6,811 factories and 259 points were selected from 1,511 recycling business points. Traffic-related facility areas were divided between gas stations, bus depots, and auto mechanics. Thirty-four points were selected from 149 bus depots and 573 points were selected from 6,013 auto mechanic points. From the 2,409 gas station points, 323 were selected. Conclusion: Contaminated soil influences groundwater and crops, which can harm human health. However, soil pollution is not easily identified, so it is difficult to determine what has occurred. Pollution must be prevented beforehand and contaminated soil found. By selecting and investigating soil contamination survey points in consideration of the location of groundwater wells, we can safely manage water resources by preventing groundwater contamination in advance.