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      • KCI등재

        일회용 위생장갑에서 Phthalate류 및 Di-(2-ethylhexyl) adipate 분석

        이광호,권기성,곽인신,최재천,전대훈,정동윤,최병희,김성욱,이선희,이철원,Lee, Kwang-Ho,Kwon, Ki-Sung,Kwak, In-Shin,Choi, Jae-Chon,Jeon, Dae-Hoon,Jeong, Dong-Youn,Choi, Byung-Hee,Kim, Sung-Wook,Lee, Sun-Hee,Lee, Chul-Won 한국포장학회 2000 한국포장학회지 Vol.6 No.1

        일회용 위생장갑에서 diethyl phthalate (DEP), di-n-propyl phthalate (DprP), di-n-butyl phthalate (DBP), di-n-pentyl phthalate (DPP), butylbenzyl phthalate (BBP), di-(2-ethylhexyl) phthalate (DEHP) 및 dicyclohexyl phthalate (DCHP) 등과 같은 phthalate ester 와 di-(2-ethylhexyl) adipate (DEHA) 을 분석하였다. 일회용 위생장갑은 소매점에서 구입하였으며, 사염화탄소를 추출용매로 6시간 동안 Soxhlet 장치에서 추출하였다. 8종의 제품 모두 poly-ethylene (PE) 재질이었으며, 식품위생법에 따라 box 포장에 표기 사항이 있었다. 8 종의 모든 제품에서 Phthalate ester 류 와 DEHA는 검출한계를 넘지 않았다. Phthalate esters 인 DEP, DprP, DBP, DPP, BBP, DEHP, DCHP와 DEHA의 검출한계는 각각 1.8, 1.9, 1.3, 1.1, 0.9, 0.7, 2.1 와 0.8 mg/L 이었다. The level of plasticizer such as diethyl phthalate (DEP), di-n-propyl phthalate (DprP), di-n-butyl phthalate (DBP), di-n-pentyl phthalate (DPP), butylbenzyl phthalate (BBP), di-(2-ethylhexyl) phthalate (DEHP), dicyclohexyl phthalate (DCHP) and di-(2-ethylhexyl) adipate (DEHA) was determined in disposable sanitary gloves. Samples of disposable sanitary gloves were taken at retail shops, and their overall extractions in carbon tetrachloride were measured, after establishment of soxhlet appratus in 6 hours. All of 8 samples of disposable sanitary gloves at retail shops were polyethylene (PE). All of the manufactures was voluntarily labelled their boxes of gloves in line Korea Food Code. The level of phthalate esters and DEHA in all of 8 samples were not exceed the detection limit. The detection limits of DEP, DprP, DBP, DPP, BBP, DEHP, DCHP and DEHA were 1.8, 1.9, 1.3, 1.1, 0.9, 0.7, 2.1 and 0.8 mg/L, respectively.

      • KCI등재

        스피넬계 흑색 안료를 이용한 흑색 지르코니아 세라믹스의 제조 및 특성분석

        이광호,이용석,박주석,이병하,Lee, Kwang-Ho,Lee, Yong-Seok,Park, Joo-Seok,Lee, Byung-Ha 한국세라믹학회 2008 한국세라믹학회지 Vol.45 No.4

        The zirconia ceramics are widely used because of their excellent mechanical properties. Recently, many researches to make a colored zirconia was achieved to satisfy the individual aesthetic requirements. In this study, the synthesis of black-color spinel-based inorganic pigments which are stable above $1400^{\circ}C$ and the fabrication of black-colored zirconia using the synthesized pigments are investigated. Inorganic pigments which have spinel structure and near black color were synthesized by a solid state reaction method using a $Fe_2O_3,\;Cr_2O_3$, CoO and NiO powder as a starting materials at $1600^{\circ}C$. Most of synthesized pigments were black colored spinel phases and single spinel phase was successfully synthesized at the composition range of $Cr_2O_3:25{\sim}35%,\;Fe_2O_3:45{\sim}55%$, CoO:20% and NiO:$6{\sim}10%$. The black-colored zirconia was fabricated at $1410^{\circ}C$ with the 5 wt% synthesized pigments and their properties were evaluated. The results showed that the strength value was more than 848 MPa, absorption rate was 0.1%, the brightness of color was $L^*:40{\sim}42$, the tone of color is $a^*:0.2{\sim}0.8$ and $b^*:-1.1{\sim}2.4$. As a result, the black-colored zirconia was suitable for a artificial jewelry or decoration zirconia goods.

      • KCI등재

        흑연 함침법에 의한 흑색 지르코니아의 제조 및 특성분석

        이광호,안종필,박주석,이용석,이병하,Lee, Kwang-Ho,Ahn, Jong-Pil,Park, Joo-Seok,Lee, Yong-Seok,Lee, Byung-Ha 한국세라믹학회 2009 한국세라믹학회지 Vol.46 No.4

        Zirconia is widely used for structural materials in machinery due to its superior properties, such as high strength, high hardness, and high toughness. Zirconia generally has ivory or white color. Therefore many studies are performed for diversification of zirconia color, in order to be widely uitilized for decoration and machine parts which need distincfive color. In this study, graphite is used to prevent structural defect, to maintain superior properties, and to develop black color of zirconia by impregnation method. As specimen was impregnated at $1600^{\circ}C$ for 2 h, bending strength is 1221 MPa, density is $6.01\;g/cm^3$, hardness is 10.1 GPa, absorption coefficient is 0%, transmittance is Fail, chromaticity is 54. The results indicate that black zirconia has enough properties to be adopted as mechanical parts. Optimum impregnation time is 2 h for various observations.

      • KCI등재

        황동제 주방기구에서 유해중금속의 용출기작에 관한연구

        이광호,권기성,전대훈,최병희,김성욱,이선희,이철원,Lee, Kwang-Ho,Kwon, Ki-Sung,Jeon, Dae-Hoon,Choi, Byung-Hee,Kim, Sung-Wook,Lee, Sun-Hee,Lee, Chul-Won 한국포장학회 1999 한국포장학회지 Vol.5 No.2

        구이용 불판인 주방용 기구에 사용되는 황동제에서 Pb, Cd, Cu, Zn, Sn등 유해 중금속의 용출과 메카니즘에 대하여 연구하였다. 황동을 대표금속으로 선정하여 용출 온도 (30, 60, 80, $95^{\circ}C$), pH (2.5, 4.3, 6.0, 7.0) 및 시간 (30, 90, 180, 360분)에 따른 금속 용출량 조사에서 온도 및 pH 변화에 따른 시험결과, $95^{\circ}C$, pH 2.5인 조건에서 용출이 가장 많았던 반면, 용출 시간별 시험에서는 180분 이후까지 Pb가 용출된 후 평형 상태를 유지하였다. 납이 용출되는 가시적 현상은 SEM을 통하여 확인할 수 있었다. 황동의 경우, 재질중의 Pb 함량과 용출량과의 관계를 규명하기 위해 Pb 함량별 10종 (0, 0.02, 0.09, 0.1, 0.2, 0.5, 0.9, 1.7, 5.4, 9.2%(w/w))의 시편를 제작하여 4% 초산, $95^{\circ}C$, 30분에서 시험한 결과, 용출규격인 중금속이 1.0 ppm (납으로서) 이하가 되기 위해서는 재질중 허용 Pb 함량은 0.2% 이하가 되어야 했다. The migration mechanism of trace elements, Pb, Cd, Cu, Zn and Sn from brass food-contact utensiles was investigated. The migration of metals from brass was affected by the migration temperature (30, 60, 80 and $95^{\circ}C$), the simulant pH (2.5, 4.3, 6.0 and 7.0) and the migration time (30, 90, 180 and 360 min.). The amount of Pb migration was maximum at $95^{\circ}C$ with pH 2.5. This study indicated that the equilibrium of Pb migration was reached at 180 minutes. The mechanism of Pb migration was investigated with Scanning Electron Microscope (SEM) and Electron Probe Micro Analyzer (EPMA). To correlate the relations between the migration and the content of Pb in brass samples, ten brass samples having known content of Pb (the quantities of Pb in brass ; 0, 0.02, 0.09, 0.1, 0.2, 0.5, 0.9, 1.4, 5.4 and 9.2% (w/w)) were tested in the following conditions, 4% acetic acid, $95^{\circ}C$ and 30 minutes. The result represented that content of Pb in brass samples must be below 0.2% (w/w) to satisfy the 1.0 ppm (as Pb) of Korea Food Code.

      • KCI등재

        해안안벽과 육상구조물에서 지진해일파의 처오름 및 작용파력에 관한 수치해석

        이광호,김창훈,김도삼,황용태,Lee, Kwang Ho,Kim, Chang Hoon,Kim, Do Sam,Yeh, Harry,Hwang, Young Tae 대한토목학회 2009 대한토목학회논문집 B Vol.29 No.3B

        In this work, wave run-up heights and resultant wave forces on a vertical revetment due to tsunami (solitary wave) are investigated numerically using a numerical wave tank model called CADMAS-SURF (CDIT, 2001. Research and Development of Numerical Wave Channel (CADMAS-SURF). CDIT library, No. 12, Japan.), which is based on a 2-D Navier-Stokes solver, coupled to a volume of fluid (VOF) method. The third order approximate solution (Fenton, 1972. A ninth-order solution for the solitary wave. J. of Fluid Mech., Vol. 53, No.2, pp.257-271) is used to generate solitary waves and implemented in original CADMAS-SURF code. Numerical results of the wave profiles and forces are in good agreements with available experimental data. Using the numerical results, the regression curves determined from the least-square analysis are proposed, which can be used to determine the maximum wave run-up height and force on a vertical revetment due to tsunami. In addition, the capability of CADMAS-SURF is demonstrated for tsunami wave forces acting on an onshore structure using various configuration computations including the variations of the crown heights of the vertical wall and the position of the onshore structure. Based on the numerical results such as water level, velocity field and wave force, the direct effects of tsunami on an onshore structure are discussed. 본 연구에서는 Navier-Stokes방정식과 자유수면추적을 위해 도입한 VOF함수의 이류방정식에 기초하고 있는 CADMAS-SURF(CDIT, 2001)에 Fenton(1972)의 3차근사고립파이론에 의한 조파이론을 새롭게 도입한 수치파동수로로부터 직립호안상에서 지진해일(고립파)의 처오름 및 작용파력을 해석한다. 기존의 연구결과와 대비하여 본 수치해석결과의 적용성을 논의하며, 최소자승법에 기초하여 직립호안상에서 최대처오름과 최대파력을 합리적으로 추정할 수 있는 회귀식을 제안한다. 또한, 육상구조물에 작용하는 지진해일(tsunami wave)의 파력산정에 CADMAS-SURF(CDIT, 2001)의 적용을 시도한다. 육상에서 지진해일의 수위변동, 유속 및 파력변동의 특성으로부터 육상구조물에 미치는 지진해일의 직접적인 영향을 추론할 수 있을것이다.

      • 매선료법(埋線療法)에 대한 문헌적(文獻的) 고찰(考察)

        이광호,이동희,권기록,박희수,박영엽,Lee, Kwang-Ho,Lee, Dong-Hee,Kwon, Ki-Rok,Park, Hee-Soo,Park, Yong-Yup 대한약침학회 2003 Journal of pharmacopuncture Vol.6 No.3

        Background : This study focuses on the new acupuncture method of embedding method which inserts a substance on the acupuncture points for continuous stimulation. Clinical applications and cautions were examined through literary investigations. Results : Based on the literary consideration of embedding method, the following results were obtained : 1. Embedding method is a combination of traditional and embedding technique to provide longer duration of stimulation on the acupuncture points. 2. To administer the embedding method, one needs to utilize a embedding thread besides acupuncture apparatus. Sheep gut is commonly used in China and the surgical thread is the choice in Korea. 3. Embedding method may vary from the patient to patient, depending on the nature and location of the illness. Piercing, embedding, and tying are some of the possibilities. 4. Embedding method may have different arrangement of threads based on the choice of usage. 5. Embedding method is effective for various chronic illnesses such as aches, functional diseases, and the diseases of internal organs. 6. When using the embedding methods, cautions against infection and side effects due to strong stimulation are mandatory.

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