부분 오스테나이트화 후 항온 변태한 1.0C-1.5Cr 베어링강의 미세조직 특성

윤동주,최병영 ( Dong Joo Yoon,Byung Young Choi ) 한국열처리공학회 1996 熱處理工學會誌 Vol.9 No.1

Metallographic observation was carried out by scanning and transmission electron microscopy to evaluate microstructural characteristics of partially austenitized and isothermally transformed 1.0C-1.5Cr bearing steel. It was observed that lower bainite formed in the local region of specimen partially austenitized and isothermally held at 250℃ for 1/3hr and formed in almost all area of the specimen isothermally held at 250℃ for 2hrs. Lower bainitic carbides with midrib was also observed in the specimen partially austenitized and isothermally held at 250℃ for 4hrs. Midrib was nearly carbide-free region and thicker in the vicinity of spherical carbides than the other region. Lengthening speed of lower bainitic carbides was remarkabey increased at isothermal holding time ranging from 2hrs to 4hrs.

고정성 보철물을 지지하는 골유착성 임플란트의 위치에 따른 지지조직에서의 유한요소적 응력분석

윤동주,신상완,서규원,Yoon, Dong-Joo,Shin, Sang-Wan,Suh, Kyu-Won 대한치과보철학회 1993 대한치과보철학회지 Vol.31 No.1

Many studies have been reported on the successful replacement of missing teeth with osseointegrated dental Implants. However, little research has been carried out on the bio-mechanical aspect of the stress on the surrounding bone of the free-standing type of dental implant prostheses. This experimental study was aimed to analyze the stress distribution pattern on the supporting tissues depending upon the position of osseointegrated implants supporting fixed bridges. In the cases of unilateral partially edentulous mandible (the 2nd premolar and the 1st and 2nd molars missing), two osseointegrated implants were placed at the 2nd premolar and 2nd molar sites (Model A) , the 1st and 2nd molar sites (Model B, Anterior cantilevered type), the 2nd premolar and 1st molar sites (Model C, Posterior cantilevered type). Chewing forces of dentate patients and denture wearer were applied vertically on the 2nd premolar, the 1st molar, and the 2nd molar of each model. A 3-Unit fixed partial denture was constructed at each model and cantilevered extension parts were involved in Model B and Model C. Two dimensional finite element analysis was undertaken. The commercial software (Super SAP) for IBM 16 bit personal computer was utilized. The results were as follows : 1. The magnitude of applied load influenced on the total value of stresses, but did not in-fluence on the pattern of stress distribution. 2. The magnitude of stress developed from the supporting tissues were in order of Model C,Model A,Model B. 3. High stresses were concentrated on the cervical and apical portion of the implant/bone interface. 4. A difference of the stress magnitude on the implant/bone interface between mesial and distal implant was most prominant in Model C and in order of Model A and Model B. 5. The stresses developed in Model A were evenly distributed throughout both implants. 6. The stresses concentrated on the cervical portion of cantilevered side were higher in the posterior cantilevered type than in the anterior cantilevered type.

강화형 간접복합레진과 치과용 합금의 결합강도에 관한 연구

윤동주,신상완,임호남,서규원,Yoon, Dong-Joo,Shin, Sang-Wan,Lim, Ho-Nam,Suh, Kyu-Won 대한치과보철학회 1999 대한치과보철학회지 Vol.37 No.5

Indirect composite resins are used as an popular effective esthetic material in prosthetic dentistry, often with metallic substructure that provides support for restorations. Recently, new indirect composite resins as a substitute of ceramic have been developed. These resins provide good esthetics, with a wide range of hue and chroma. And the flexural strength of those is in the range of 120-150MPa, Which is higher than that of feldspathic Ceramic, and similar th that of Dicor. Although it has many merits, one of the major clinical problems of composite resins is the bond failure between metal and resin due to insufficient interfacial bond strength. The purpose of this study was to evaluate shear bond strength of the reinforced indirect composite resin to dental alloys. Three different composite resin systems($Artglass^{(R)},\;Sculpture^{(R)},\;Targis^{(R)}$) as test groups and ceramic($VMK\;68^{(R)}$) as control group were bonded to Ni-Cr-Be alloy($Rexillium\;III^{(R)}$) and gold alloy(Deva 4). All specimens were stored at $^37{\circ}C$ distilled water for 24 hours and the half of specimens were thermocycled 2000 times at temperature from $5^{\circ}C\;to\;60^{\circ}C$. The shear bond strengths of reinforced indirect composite resins to dental alloys were measured by using the universal testing machine, and modes of debonding were observed by stereoscope and scanning electron microscope. The results were as follows: 1 The shear bond strengths of reinforced indirect composite resins to dental alloys were approximately half those of ceramic to dental alloys(P<0.01). 2. There was no significant difference between the shear bond strength of several reinforced indirect composite resins to metal. 3. Alloy type did not affect on the shear bond strengths of resin to metal, but the shear bond strengths of ceramic to gold alloys were higher than those of ceramic to Ni-Cr alloys(P<0.05). 4. The shear bond strengths of Artglass and Targil to gold alloys were significantly decreased after thermocycling treatment(P<0.01). 5. Sculpture showed cohesive, adhesive, and mixed failure modes, but Artglass and Targis showed adhesive or mixed failures. And ceramic showed cohesive and mixed failures.

콘크리트 거동의 수분-열적, 화학-역학적, 환경적 연계반응에 관한 연구

윤동주(Yoon Dong-Ju),송하원(Song Ha-Won),김성훈(Kim Sung-Hoon),변근주(Byun Keun-Joo) 대한토목학회 2000 대한토목학회 학술발표회 논문집 Vol.2000 No.1

DV-Xα 분자궤도법으로 설계한 생체용 Ti-Ag-Zr 합금 특성 평가

백민숙,윤동주,김병일,Baek, Min-Sook,Yoon, Dong-Joo,Kim, Byung-Il 한국재료학회 2014 한국재료학회지 Vol.24 No.4

Ti and Ti alloys have been extensively used in the medical and dental fields because of their good corrosion resistance, high strength to density ratio and especially, their low elastic modulus compared to other metallic materials. Recent trends in biomaterials research have focused on development of metallic alloys with elastic modulus similar to natural bone, however, many candidate materials also contain toxic elements that would be biologically harmful. In this study, new Ti based alloys which do not contain the toxic metallic components were developed using a theoretical method (DV-$X{\alpha}$). In addition, alloys were developed with improved mechanical properties and corrosion resistance. Ternary Ti-Ag-Zr alloys consisting of biocompatible alloying elements were produced to investigate the alloying effect on microstructure, corrosion resistance, mechanical properties and biocompatibility. The effects of various contents of Zr on the mechanical properties and biocompatibility were compared. The alloys exhibited higher strength and corrosion resistance than pure Ti, had antibacterial properties, and were not observed to be cytotoxic. Of the designed alloys' mechanical properties and biocompatibility, the Ti-3Ag-0.5Zr alloy had the best results.

AIP법으로 증착된 TiN/CrN 다층박막의 특성 분석

백민숙,윤동주,허기복,김병일,Baek, Min-Sook,Yoon, Dong-Joo,Heo, Ki-Bok,Kim, Byung-Il 한국재료학회 2018 한국재료학회지 Vol.28 No.7

TiN and CrN thin films are among the most used coatings in machine and tool steels. TiN and CrN are deposited by arc ion plating(AIP) method. The AIP method inhibits the reaction by depositing a hard, protective coating on the material surface. In this study, the characteristics of multi-layer(TiN/CrN/TiN(TCT), CrN/TiN/CrN(CTC)) are investigated. For comparison, TiN with the same thickness as the multilayer is formed as a single layer and analyzed. Thin films formed as multilayers are well stacked. The characteristics of micro hardness and corrosion resistance are better than those of single layer TiN. The TiN/CrN peak is confirmed because both TCT and CTC are formed of the same component(TiN, CrN), and the phase is first grown in the (111) direction, which is the growth direction. However, the adhesion and abrasion resistance of the multilayer films are somewhat lower.

프리스트레스트 콘크리트 포장의 횡방향 긴장 설계방안

김성민,윤동주,배종오,Kim, Seong-Min,Yoon, Dong-Joo,Bae, Jong-Oh 한국도로학회 2008 한국도로학회논문집 Vol.10 No.4

본 연구는 프리스트레스트 콘크리트 포장(PSCP)의 횡방향 긴장 설계방안을 구축하기 위하여 수행되었다. 우선 PSCP에 횡방향 긴장을 가했을 경우에 긴장간격에 따른 슬래브의 응력분포를 분석하였다. 또한 환경하중과 차륜하중이 PSCP슬래브에 작용할 때 슬래브에 발생하는 인장응력의 분포도 분석하였다. 이러한 환경 및 차륜하중 등의 설계하중과 긴장응력을 결정하는 기준인 슬래브의 허용인장응력을 합리적으로 선정하는 방법에 대하여 논의하였으며 이러한 기준의 선정이 횡방향 긴장 설계에 미치는 영향을 분석하였다. 연구결과, 긴장간격이 커질수록 긴장응력의 손실을 가져오는 범위가 넓어지며 특히 Shoulder부분에서의 응력손실이 급격하게 증가하는 것을 알 수 있었다. 따라서 횡방향 긴장 설계는 설계하중에 대한 슬래브의 응력을 산출한 후 슬래브가 허용인장응력 이내의 응력을 받도록 평균긴장응력을 산출하여 긴장간격 및 긴장량을 결정하면 되지만, 이때 Shoulder, Wheel Pass, 중앙부 등 슬래브의 여러 다른 위치에서의 응력 또한 반드시 검토하여 적절한 긴장간격을 선정하여야 한다. This study was conducted to develop the design methodology of transverse post-tensioning for the prestressed concrete pavement (PSCP). The transverse stress distribution was analyzed when the transverse anchor spacing changed. The tensile stress distribution in the PSCP slab due to the environmental and vehicle loads was also investigated. The reasonable methods were discussed to determine the design loads including environmental and vehicle loads and the PSCP allowable tensile stress used for the basis of the selection of the stress application amount from the tensioning. The results of this study showed that as the transverse anchor spacing increased, the range of the stress loss became larger and the stress loss was significant near the shoulder. The design of the transverse post-tensioning can be performed by obtaining the stresses under the design loads and by considering the allowable tensile stress; however, the tensile stresses at different locations such as the shoulder, wheel pass, and slab interior should also be checked and kept below the allowable tensile stress.

AIP법으로 형성된 TiAgN 코팅필름의 바이어스전압에 따른 표면 특성 분석

백민숙,윤동주,강병모,정운조,김병일,Baek, Min-Sook,Yoon, Dong-Joo,Kang, Byeong-Mo,Jeong, Woon-Jo,Kim, Byung-Il 한국재료학회 2015 한국재료학회지 Vol.25 No.5

The implanting of metal products is performed with numerous surface treatments because of toxicity and adhesion. Recently, the surface modification of metal products has been actively studied by coating the surface of the TiC or TiN film. We prepared a Ti(10%)Ag Target which may be used in dental oral material by, using the AIP(arc ion plating) system TiAgN coating layer that was deposited on Ti g.23. The purpose of this study was to establish the optimal bias voltage conditions of the coated TiAgN layer formed by the AIP process. The TiAgN coatings were prepared with different bias voltage parameters (0V to -500V) to investigate the effect of bias voltage on their mechanical and chemical properties. The SEM(scanning electron microscope), EDS(energy dispersive X-ray spectrometer), XRD(X-ray diffraction), micro-hardness, and potentiodynamic polarization were measured and the surface characteristics of the TiAgN coating layers were evaluated. The TiAgN coating layer had different mechanical characteristics based on the bias voltage, which also showed differences in thickness and composition.

횡방향 긴장에 의한 프리스트레스트 콘크리트 포장의 거동분석

김성민,윤동주,김동호,Kim, Seong-Min,Yoon, Dong-Joo,Kim, Dong-Ho 한국도로학회 2008 한국도로학회논문집 Vol.10 No.4

본 연구에서는 프리스트레스트 콘크리트 포장에 횡방향으로 프리스트레싱을 가할 때 포장체에 발생하는 응력분포를 분석하여 긴장간격에 따른 특성을 파악하고 종방향과 횡방향 긴장의 상호 영향을 분석하기 위하여 유한요소 모델을 개발하여 구조해석을 수행하였다. 연구결과 횡방향 긴장간격은 작을수록 응력분배를 적절하게 할 수 있고 압축응력의 손실범위를 줄일 수 있으나 경제성 문제를 제고하여 적절한 긴장간격을 선정하여야 한다. 포장체의 노견, 주행위치, 중앙부 등의 여러 위치에서 분석한 횡방향 응력분포는 긴장간격이 넓을수록 평균응력과의 차이가 커지며 그 차이는 슬래브 중앙부로 갈수록 감소하게 된다. 횡방향 긴장을 가하면 종방향으로도 추가 긴장력 이 발생하게 되지만 그 크기는 무시 할 수 있을 정도로 작기 때문에 종횡방향 긴장 설계는 독립적으로 수행하여도 타당하다. 또한 횡방향 긴장 설계 시 이러한 긴장에 의한 응력분포를 이용하는 방안에 대해서도 본 논문에 언급하였다. This study was conducted to investigate the stress distribution in the prestressed concrete pavement (PSCP) when the transverse post tensioning was applied. By performing the structural analyses using a finite element model of PSCP, the effect of anchor spacing and the relationship between the longitudinal and transverse post tensioning were evaluated. The analysis results showed that as the anchor spacing became smaller, the stresses were more uniformly distributed and the ranges of the stress losses were reduced; however, the economy should be considered. As the anchor spacing became larger, the difference between the average transverse stress and the transverse stresses at various locations such as shoulder, wheel pass, and center of the slab, increased. The transverse post tensioning induced the additional tensile forces in the longitudinal tendons, but the magnitude was negligibly small, and the longitudinal and transverse post tensioning could be designed independently. The use of the transverse stress distribution for the design of the post tensioning was also discussed in this paper.

양극산화와 열수처리한 니오비움 금속의 표면특성

원대희,김영순,윤동주,이민호,배태성,Won Dae-Hee,Kim Young-Soon,Yoon Dong-Joo,Lee Min-Ho,Bae Tae-Sung 한국재료학회 2005 한국재료학회지 Vol.15 No.2

This study was performed to investigate the surface properties of electrochemically oxidized pure niobium by anodic oxide and hydrothermal treatment technique. Niobium specimens of $10mm\times10mm\times1.0mm$ in dimension were polished sequentially from $\#600,\;\#800,\;\#1000$ emery paper. The surface of pure niobium sperimens was anodized in an electrolytic solution that was dissolved calcium and phosphate in water. The electrolytic voltage was set in the range of 250 V and the current density was $10mA/cm^2$. The specimen was hydrothermal treated in high-pressure steam at $300^{\circ}C$ for 2 hours using an autoclave. And all specimens were immersed in the in the Hanks' solution nth pH 7.4 at $37^{\circ}C$ for 30 days. The surface of specimen was characterized by surface roughness, scanning electron microscope(SEM), energy dispersion X-ray analysis(EDX), X-ray photoemission spectroscopy(XPS) test. The value of surface roughness was the highest in the anodized sample and $0.41{\pm}0.04\;{\mu}m$. The results of the SEM observation show that oxide layers of the multi porosity in the anodized sample were piled up on another, and hydroxyapatite crystal was precipitate from the surface of the hydrothermal treated sample. In the XPS analysis, O, Nb, C peak and small amounts of N peak were found in the polished specimens while Ca and P peak in addition to O, Nb, C and peak were observed in the hydrothermal treated sample.