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Styrene과 2-Hydroxypropylacrylate(2-HPA) 공중합 특성
박근호,정영언,김남석,설수덕,서영옥 東亞大學校 大學院 1999 大學院論文集 Vol.24 No.-
Solution copolymerization of Styrene(St.) with 2-Hydroxypropylacrylate(2-HPA) was carried out with Benzoylperoxide(BPO) as an initiator in toluene at 80℃ in a batch reactor. Reaction volume and reaction time were 0.3 liters, 7hours respectively. The time to reach steady state was about the six time. The monomer reactivity ratios, r1(St.) and r2(2HPS) were determined by both the Kelen-Tudos method and the Fineman-Ross method : r1(St.)=0.376(0.330), r2(2-HPA)=0.408(0.778). The activation energy of thermal decomposition was in range of 33∼55 kcal/mol.