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A study of thermolysis of irradiated diamide-containing extraction systems with nitric acid
I.V. Srvortsov,E.V. Belova,I.P. Sokolov,A.V. Rodin,S.V. Stefanovsky,B.F. Mysoedov 한국원자력학회 2018 Nuclear Engineering and Technology Vol.50 No.8
The dynamics of gas release at thermal oxidation of extraction systems on the basis of diamides ofdicarbonic acids in fluorinated sulphones with 14 mol/L HNO3 was investigated. The effect of preirradiationof the mixtures with accelerated electrons on the kinetics of their thermolysis was determined. The mixtures were heated in an autoclave at temperatures of 170 and 200 C and irradiated usingan electron accelerator to absorbed doses of 0.1, 0.5, and 1.0 MGy. It has been shown that no conditionsfor autocatalytic oxidation at thermolysis of extraction mixtures irradiated up to a dose of 1 MGy weredeveloped.