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RISS 인기검색어
- 검색키워드
- 저자 : Miranda Lima Rose (검색결과 6 건)
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E. Padmini.,M. Helen Kalavathy,Miranda Lima Rose 한국탄소학회 2008 Carbon Letters Vol.9 No.2
In the present study Sisal fiber obtained from the leaves of Agave sisalana has been chosen to validate its viability as an adsorbent for the removal of Nickel from aqueous solutions. The material was also surface modified and its effect on adsorption of Nickel was also studied. Agave sisalana fiber was found to be a cheap and effective adsorbent doing away with the need to activate the material therby reducing processing cost. The equilibrium studies indicated that the adsorption capacity of raw fiber and the surface modified fiber was 8.66 and 9.77 mg/g respectively with the Langmuir isotherm describing the adsorption phenomena better than the Freundlich and Temkin isotherm. The adsorption was found to be exothermic from the thermodynamic studies and the kinetics showed that the adsorption phenomena were second order.
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Moringa Oleifera, A Biosorbent for Resorcinol Adsorption-Isotherm and Kinetic Studies
M. Helen Kalavathy,G. Swaroop,E. Padmini,Miranda Lima Rose 한국탄소학회 2009 Carbon Letters Vol.10 No.1
The adsorption of phenolic compound resorcinol on activated carbons prepared from Moringa oleifera (Drumstick bark) has been investigated. Activated carbon was prepared by impregnating Moringa oleifera with 50% phosphoric acid in the ratio of 1:1 and 1:2(w/w), designated as MOAC1 and MOAC2. Equilibrium and isotherm studies were carried out. The influences of variables such as contact time, initial concentration of resorcinol, carbon dosage in the solution on percentage adsorption and adsorption capacity of the bark have been analysed. The equilibration time was found to be 4 h. Kinetics of resorcinol onto activated carbons was checked for pseudo first order and pseudo second order model. It was found that the adsorption of resorcinol follows pseudo second order kinetics for both MOAC1 and MOAC2. The isotherm data were correlated with isotherm models, namely Langmuir and Freundlich. Adsorption isotherms were satisfactorily fitted by both the Langmuir and Freundlich model for MOAC1 and MOAC2.
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E. Padmini.,Singh K. Prakash,Lima Rose Miranda 한국탄소학회 2010 Carbon Letters Vol.11 No.4
The photodegradation of the model compounds Quinol, an aromatic organic compound and Acid blue FFS, an acid dye of chemical class Triphenylmethane was studied by using illumination with UV lamp of light intensity 250W. TiO2 and TiO2 doped with Boron and Nitrogen was used as catalyst. The sol-gel method was followed with titanium isopropoxide as precursor and doping was done using Boron and Nitrogen. In photocatalytic degradation, TiO2 and doped TiO2 dosage, UV illumination time and initial concentration of the compounds were changed and examined in order to determine the optimal experimental conditions. Operational time was optimized for 360 min. The optimum dosage of TiO2 and BN doped TiO2 was obtained to be 2 mgL-1 and 2.5 mgL-1 respectively. Maximum degradation % for quinol and Blue FFS acid dye was 78 and 95 respectively, at the optimum dosage of BN-doped TiO2 catalyst. It was 10 and 4% higher than when undoped TiO2 catalyst was used.
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Padmini. E,Helen Kalavathy M,Lima Rose Miranda 한국탄소학회 2008 Carbon Letters Vol.9 No.2
In the present study Sisal fiber obtained from the leaves of Agave sisalana has been chosen to validate its viability as anadsorption of Nickel was also studied. Agave sisalana fiber was found to be a cheap and effective adsorbent doing away withthe need to activate the material therby reducing processing cost. The equilibrium studies indicated that the adsorptioncapacity of raw fiber and the surface modified fiber was 8.66 and 9.77 mg/g respectively with the Langmuir isothermdescribing the adsorption phenomena better than the Freundlich and Temkin isotherm. The adsorption was found to beexothermic from the thermodynamic studies and the kinetics showed that the adsorption phenomena were second order.
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Steam Activated Carbon Preparation Using HTFBR from Biomass and its Adsorption Characteristics
J. Herbert Asirvatham,Nikhar Gargieya,Manali Sunil Paradkar,B.G. Prakash Kumar,Miranda Lima Rose 한국탄소학회 2008 Carbon Letters Vol.9 No.3
The objective of this work is to study the feasibility of the preparation of the activated carbon (AC) from coconut tree flowers using high temperature fluidized bed reactor (HTFBR). The activating agent used in this work is steam. The reactor was operated at various activation temperature (650, 700, 750, 800 and 850℃) and activation time (30, 60, 120 and 240 min) for the production of AC from coconut tree flowers. Effect of activation time and activation temperature on the quality of the AC preparation was observed. Prepared AC was characterized in-terms of iodine number, methylene blue number, methyl violet number, ethylene glycol mono ethyl ether (EGME) surface area and SEM photographs. The best quality of AC from coconut tree flowers (CFC) was obtained at an activation temperature and time of 850℃ and 1 hr restectively. The effectiveness of carbon prepared from coconut tree flowers in adsorbing crystal violet from aqueous solution has been studied as a function of agitation time, carbon dosage, and pH. The adsorption of crystal violet onto AC followed second order kinetic model. Adsorption data were modeled using both Langmuir and Freundlich classical adsorption isotherms. The adsorption capacity qm was 277.78 mg/g., equilibrium time was found to be 180 min. This adsorbent from coconut tree flowers was found to be effective for the removal of CV dye.
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Manikandan Gomathy Nainar,Kalidass Jayaraman,Helen Kalavathy Meyyappan,Lima Rose Miranda 한국화학공학회 2020 Korean Journal of Chemical Engineering Vol.37 No.12
Poly(vinylidene fluoride) (PVDF) was incorporated in Cellulose acetate (CA) to prepare polymeric blend membrane to enhance the antifouling properties and rejection. Blend membranes consist of different concentrations (0, 2.5 and 5.0 wt%) of polyvinylpyrrolidone (PVP), which was the hydrophilic polymer additive and pore forming agent. The existence of membrane functional groups was analyzed by ATR-FTIR spectroscopy. AFM and SEM were conducted to explain the surface morphology of the synthesized blend membranes. Membrane properties were examined by contact angle, porosity and equilibrium water content (EWC). The membrane’s thermal and mechanical properties were determined by performing TGA and tensile test. Membrane performance was assessed by pure water flux (PWF), rejection, antifouling properties using bovine serum albumin (BSA) and Sodium alginate (SA) solution. In this study, CPA-2 membrane showed high PWF of 269.82 L m2 h1, flux recovery ratio (FRR) against BSA and SA was 94% and 92%, respectively. Rejection of BSA and SA was found to be 83% and 86%, respectively. From the results, it was significant that the hydrophilic additive PVP blended membrane ameliorated and showed better results in surface roughness, hydrophilicity, thermal and mechanical stability. Hence, CPA-2 membrane would exhibit less susceptibility to fouling with enhanced PWF, permeability and selectivity.
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