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HARUYA OKIMOTO,WILHELM HEMME,YASUHIRO ITO,TOSHIKI SUGAI,HELLMUT ECKERT,RYO KITAURA,RYO KITAURA,HISANORI SHINOHARA 성균관대학교(자연과학캠퍼스) 성균나노과학기술원 2008 NANO Vol.3 No.1
Sc2C2@C82(II) and Sc2C2@C82(III) have been synthesized and chromatographically isolated and characterized by using UV-Vis-NIR absorption spectroscopy. Solid-state 13C and 45Sc NMR on Sc2C2@C82 metallofullerenes provide the rotational activation energy of Sc atoms encapsulated in C82 fullerenes which is lower than that in solution due to crystal field effects on the rate of the rotation.